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Production method of high-strength and high-compactness fused quartz
The invention discloses a production method of high-strength and high-compactness fused quartz. The production method comprises the following steps: (1) producing a fused quartz raw material; (2) preparing slurry, namely performing ball milling on the fused quartz raw material and cordierite by adopting a ball mill at the rotating speed of 250-300r/min in a forward and reverse ball milling mannerfor 6-10h, sieving the powder by using a 500-mesh sieve, adding the powder subjected to ball milling into a precursor solution, adding a dispersing agent, adjusting the pH value to 3-4 through lacticacid and ammonia water, and preparing slurry with the solid phase content of 60-65% through mechanical stirring; (3) conducting gel curing; (4) conducting drying; and (5) conducting microwave sintering. According to the production method of the high-strength and high-compactness fused quartz, the production method is simple and efficient, the influence of impurity elements on the chemical stability, strength and compactness of the high-strength and high-compactness fused quartz is avoided, and the prepared fused quartz has good breaking strength, high compactness, good chemical stability and wide application prospects.
一种高强高致密性熔融石英的生产方法,包括如下步骤:(1)熔融石英原料的生产;(2)料浆的制备:采用球磨机对熔融石英原料、堇青石进行球磨,转速为250‑300r/min,球磨方式采用正反转球磨,球磨时间为6‑10h,粉末过500目筛;取球墨后的粉末,加入前驱体溶液中,使得加入分散剂,通过乳酸和氨水调节pH至3‑4,通过机械搅拌制备成固相含量为60‑65%的料浆;(3)凝胶固化;(4)干燥;(5)微波烧结。本发明所述的高强高致密性熔融石英的生产方法,生产方法简单高效,避免了杂质元素对所述的高强高致密性熔融石英化学稳定性、强度、致密性的影响,制得的熔融石英具有良好的抗折强度、高致密性,化学稳定性好,应用前景广泛。
Production method of high-strength and high-compactness fused quartz
The invention discloses a production method of high-strength and high-compactness fused quartz. The production method comprises the following steps: (1) producing a fused quartz raw material; (2) preparing slurry, namely performing ball milling on the fused quartz raw material and cordierite by adopting a ball mill at the rotating speed of 250-300r/min in a forward and reverse ball milling mannerfor 6-10h, sieving the powder by using a 500-mesh sieve, adding the powder subjected to ball milling into a precursor solution, adding a dispersing agent, adjusting the pH value to 3-4 through lacticacid and ammonia water, and preparing slurry with the solid phase content of 60-65% through mechanical stirring; (3) conducting gel curing; (4) conducting drying; and (5) conducting microwave sintering. According to the production method of the high-strength and high-compactness fused quartz, the production method is simple and efficient, the influence of impurity elements on the chemical stability, strength and compactness of the high-strength and high-compactness fused quartz is avoided, and the prepared fused quartz has good breaking strength, high compactness, good chemical stability and wide application prospects.
一种高强高致密性熔融石英的生产方法,包括如下步骤:(1)熔融石英原料的生产;(2)料浆的制备:采用球磨机对熔融石英原料、堇青石进行球磨,转速为250‑300r/min,球磨方式采用正反转球磨,球磨时间为6‑10h,粉末过500目筛;取球墨后的粉末,加入前驱体溶液中,使得加入分散剂,通过乳酸和氨水调节pH至3‑4,通过机械搅拌制备成固相含量为60‑65%的料浆;(3)凝胶固化;(4)干燥;(5)微波烧结。本发明所述的高强高致密性熔融石英的生产方法,生产方法简单高效,避免了杂质元素对所述的高强高致密性熔融石英化学稳定性、强度、致密性的影响,制得的熔融石英具有良好的抗折强度、高致密性,化学稳定性好,应用前景广泛。
Production method of high-strength and high-compactness fused quartz
一种高强高致密性熔融石英的生产方法
JI MINGGUANG (Autor:in)
02.02.2021
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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