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Preparation method of intelligent self-healing admixture
The invention discloses a preparation method of an intelligent self-healing admixture, which comprises the following steps: (1) dissolving 5-10 parts of dicyclopentadiene (DCPD) in 90-95 parts of N, N-dimethylformamide (DMF) to obtain a solution A, (2) dissolving 5-10 parts of polyacrylonitrile (PAN) into 90-95 parts of N, N-dimethylformamide (DMF) to obtain a solution B, (3) carrying out coaxialelectrostatic spinning by taking the liquid A as a core layer and the liquid B as a sheath layer, wherein the fixed voltage is 15-22KV, (4) cutting the fibers obtained by electrostatic spinning in thestep (3) into short fibers with the length of 5-20mm, (5) stirring and dissolving 0.25 part of polyacrylamide in 40-45 parts of tap water to obtain a liquid C, and (6) stirring and mixing 60 parts ofthe liquid C and 40 parts of the short fibers obtained in the step (4) to obtain the intelligent self-healing admixture. When the intelligent self-healing admixture prepared by the invention is applied to concrete, the strength of a concrete building structure can be greatly enhanced.
本发明公开了一种智能自愈合外加剂的制备方法,包括以下制备步骤:(1)、将5‑10份双环戊二烯(DCPD)溶解于90‑95份N,N‑二甲基甲酰胺(DMF)中得到液A;(2)、将5‑10份聚丙烯腈(PAN)溶于90‑95份N,N‑二甲基甲酰胺(DMF)中得到液B;(3)、以液A为芯层与液B为鞘层进行同轴静电纺丝,其中固定电压为15‑22KV;(4)、将上述步骤(3)中静电纺丝得到的纤维切断为长度5‑20mm的短纤维;(5)、将0.25份聚丙烯酰胺搅拌溶解于40‑45份自来水中,得到液C;(6)、将60份液C与40份上述步骤(4)中得到的短纤维搅拌混合得到一种智能自愈合外加剂;将本发明制备的智能自愈合外加剂应用于混凝土中,能极大增强混凝土建筑结构的强度。
Preparation method of intelligent self-healing admixture
The invention discloses a preparation method of an intelligent self-healing admixture, which comprises the following steps: (1) dissolving 5-10 parts of dicyclopentadiene (DCPD) in 90-95 parts of N, N-dimethylformamide (DMF) to obtain a solution A, (2) dissolving 5-10 parts of polyacrylonitrile (PAN) into 90-95 parts of N, N-dimethylformamide (DMF) to obtain a solution B, (3) carrying out coaxialelectrostatic spinning by taking the liquid A as a core layer and the liquid B as a sheath layer, wherein the fixed voltage is 15-22KV, (4) cutting the fibers obtained by electrostatic spinning in thestep (3) into short fibers with the length of 5-20mm, (5) stirring and dissolving 0.25 part of polyacrylamide in 40-45 parts of tap water to obtain a liquid C, and (6) stirring and mixing 60 parts ofthe liquid C and 40 parts of the short fibers obtained in the step (4) to obtain the intelligent self-healing admixture. When the intelligent self-healing admixture prepared by the invention is applied to concrete, the strength of a concrete building structure can be greatly enhanced.
本发明公开了一种智能自愈合外加剂的制备方法,包括以下制备步骤:(1)、将5‑10份双环戊二烯(DCPD)溶解于90‑95份N,N‑二甲基甲酰胺(DMF)中得到液A;(2)、将5‑10份聚丙烯腈(PAN)溶于90‑95份N,N‑二甲基甲酰胺(DMF)中得到液B;(3)、以液A为芯层与液B为鞘层进行同轴静电纺丝,其中固定电压为15‑22KV;(4)、将上述步骤(3)中静电纺丝得到的纤维切断为长度5‑20mm的短纤维;(5)、将0.25份聚丙烯酰胺搅拌溶解于40‑45份自来水中,得到液C;(6)、将60份液C与40份上述步骤(4)中得到的短纤维搅拌混合得到一种智能自愈合外加剂;将本发明制备的智能自愈合外加剂应用于混凝土中,能极大增强混凝土建筑结构的强度。
Preparation method of intelligent self-healing admixture
一种智能自愈合外加剂的制备方法
GAO ZONGHONG (Autor:in) / CHEN JIE (Autor:in) / FANG SHICHANG (Autor:in) / TIAN YINGBING (Autor:in) / DENG NI (Autor:in)
12.02.2021
Patent
Elektronische Ressource
Chinesisch
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