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Preparation method of high-thermal-conductivity graphene plate
The invention relates to a preparation method of a high-thermal-conductivity graphene plate, which comprises the following steps of: S1, dissolving graphene oxide powder in aqueous carbon nanotube slurry with a certain concentration to obtain slurry in which the concentration of graphene oxide is 2-12%, the content of carbon nanotubes is 0.1-1% and the content of short carbon fibers is 0.1-2%; S2, adding 0.2-1% of a reducing agent; S3, fully stirring the slurry in a vacuum stirrer, and always controlling the temperature of the slurry to be 25 DEG C or below through water cooling; and S4, carrying out bubble elimination, molding, drying, high-temperature heat treatment graphitization, compaction and machining on the stirred composite slurry to obtain the graphene-based composite fuel cell bipolar plate with the thickness of 0.3-5mm and the thermal conductivity of more than 500W/(mK).
本发明一种高导热石墨烯板的制备方法,步骤S1,将氧化石墨烯粉体溶于一定浓度的水性碳纳米管浆料,配成浓度氧化石墨烯为2‑12%,碳纳米管含量为0.1‑1%,短切碳纤维含量为0.1‑2%的浆料;步骤S2,加入0.2‑1%的还原剂;步骤S3,将上述浆料在真空搅拌器中充分搅拌,并且通过水冷始终控制浆料温度在25℃以下;步骤S4,将搅拌好的复合浆料通过消除气泡、成型、干燥、高温热处理石墨化、压实、机加工的步骤,制备得到厚度0.3‑5mm,热导率500W/(mK)以上的石墨烯基复合燃料电池双极板。
Preparation method of high-thermal-conductivity graphene plate
The invention relates to a preparation method of a high-thermal-conductivity graphene plate, which comprises the following steps of: S1, dissolving graphene oxide powder in aqueous carbon nanotube slurry with a certain concentration to obtain slurry in which the concentration of graphene oxide is 2-12%, the content of carbon nanotubes is 0.1-1% and the content of short carbon fibers is 0.1-2%; S2, adding 0.2-1% of a reducing agent; S3, fully stirring the slurry in a vacuum stirrer, and always controlling the temperature of the slurry to be 25 DEG C or below through water cooling; and S4, carrying out bubble elimination, molding, drying, high-temperature heat treatment graphitization, compaction and machining on the stirred composite slurry to obtain the graphene-based composite fuel cell bipolar plate with the thickness of 0.3-5mm and the thermal conductivity of more than 500W/(mK).
本发明一种高导热石墨烯板的制备方法,步骤S1,将氧化石墨烯粉体溶于一定浓度的水性碳纳米管浆料,配成浓度氧化石墨烯为2‑12%,碳纳米管含量为0.1‑1%,短切碳纤维含量为0.1‑2%的浆料;步骤S2,加入0.2‑1%的还原剂;步骤S3,将上述浆料在真空搅拌器中充分搅拌,并且通过水冷始终控制浆料温度在25℃以下;步骤S4,将搅拌好的复合浆料通过消除气泡、成型、干燥、高温热处理石墨化、压实、机加工的步骤,制备得到厚度0.3‑5mm,热导率500W/(mK)以上的石墨烯基复合燃料电池双极板。
Preparation method of high-thermal-conductivity graphene plate
一种高导热石墨烯板的制备方法
ZHAO LIPING (Autor:in) / MA ZHIYUAN (Autor:in) / LI XING (Autor:in) / JIN MIN (Autor:in)
23.07.2021
Patent
Elektronische Ressource
Chinesisch
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