Eine Plattform für die Wissenschaft: Bauingenieurwesen, Architektur und Urbanistik
Eine Plattform für die Wissenschaft: Bauingenieurwesen, Architektur und Urbanistik
Preparation method of polycrystalline zirconium gemstone
The invention discloses a preparation method of polycrystalline zirconium gemstone. A specific embodiment of the method comprises the following steps: adding zirconium oxychloride into purified water for complete dissolution to obtain a zirconium oxychloride solution; generating a zirconium sulfate solid based on the zirconium oxychloride solution and sodium sulfate; dissolving the zirconium sulfate solid in purified water, adding yttrium chloride and a magnesium chloride solution, and mixing to obtain a mixed solution; adding an alkali solution into the mixed solution to completely separate out a solid precipitate; carrying out drying and pre-sintering treatment on the solid precipitate; introducing purified water, a coloring agent, a water-soluble organic dispersant, a water-soluble polymer stabilizer and the pre-sintered substance into a ball mill filled with aluminum oxide grinding balls, and carrying out homogenization grinding treatment to obtain a mixed suspension; and carrying out spray drying treatment on the mixed suspension to obtain the polycrystalline zirconium gem material. According to the embodiment, the hardness of the prepared zirconium gem is improved.
本公开的实施例公开了多晶锆宝石制备方法。该方法的一具体实施方式包括：将二氯氧化锆添加至纯净水中以进行完全溶解，得到二氯氧化锆溶液；基于二氯氧化锆溶液和硫酸钠，生成硫酸锆固体；将硫酸锆固体放置于纯净水中溶解，再添加氯化钇和氯化镁溶液进行混合，得到混合溶液；将碱溶液添加至混合溶液中以完全析出固体沉淀物；对固体沉淀物进行干燥和预烧结处理；将纯净水、着色剂、水溶性有机分散剂、水溶性聚合物稳定剂和预烧结后的物质导入装有氧化铝研磨球的球磨机中，以进行均化研磨处理，得到混合悬浮液；对混合悬浮液进行喷雾干燥处理，得到多晶锆宝石材料。该实施方式提高了所制备的锆宝石的硬度。
Preparation method of polycrystalline zirconium gemstone
The invention discloses a preparation method of polycrystalline zirconium gemstone. A specific embodiment of the method comprises the following steps: adding zirconium oxychloride into purified water for complete dissolution to obtain a zirconium oxychloride solution; generating a zirconium sulfate solid based on the zirconium oxychloride solution and sodium sulfate; dissolving the zirconium sulfate solid in purified water, adding yttrium chloride and a magnesium chloride solution, and mixing to obtain a mixed solution; adding an alkali solution into the mixed solution to completely separate out a solid precipitate; carrying out drying and pre-sintering treatment on the solid precipitate; introducing purified water, a coloring agent, a water-soluble organic dispersant, a water-soluble polymer stabilizer and the pre-sintered substance into a ball mill filled with aluminum oxide grinding balls, and carrying out homogenization grinding treatment to obtain a mixed suspension; and carrying out spray drying treatment on the mixed suspension to obtain the polycrystalline zirconium gem material. According to the embodiment, the hardness of the prepared zirconium gem is improved.
本公开的实施例公开了多晶锆宝石制备方法。该方法的一具体实施方式包括：将二氯氧化锆添加至纯净水中以进行完全溶解，得到二氯氧化锆溶液；基于二氯氧化锆溶液和硫酸钠，生成硫酸锆固体；将硫酸锆固体放置于纯净水中溶解，再添加氯化钇和氯化镁溶液进行混合，得到混合溶液；将碱溶液添加至混合溶液中以完全析出固体沉淀物；对固体沉淀物进行干燥和预烧结处理；将纯净水、着色剂、水溶性有机分散剂、水溶性聚合物稳定剂和预烧结后的物质导入装有氧化铝研磨球的球磨机中，以进行均化研磨处理，得到混合悬浮液；对混合悬浮液进行喷雾干燥处理，得到多晶锆宝石材料。该实施方式提高了所制备的锆宝石的硬度。
Preparation method of polycrystalline zirconium gemstone
多晶锆宝石制备方法
LIU MINJUAN (Autor:in)
10.09.2021
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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