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一种高密度IZTO靶材的制备方法
本发明涉及靶材技术领域,具体涉及一种高密度IZTO靶材的制备方法,所述制备方法包括如下步骤:S1原材料选择、S2氧化锌球磨、S3混合球磨、S4喷雾造粒、S5压力成型、S6靶材烧结。本发明选用特定BET值的氧化铟、氧化锡和氧化锌作为原材料,通过搅拌球磨使粉末混合均匀,经离心式喷雾造粒机干燥造成IZTO粉末,再使用等静压成型机将IZTO粉末压缩成素胚,然后在常压氧气气氛下进行烧结处理,控制升温速率和保温时间以实现高密度靶材的制备。与传统工艺相比,该方案可大幅度提高靶材的密度和均匀性,具有显著的应用价值。
The invention relates to the technical field of target materials, in particular to a high-density IZTO target material preparation method which comprises the following steps: S1, raw material selection, S2, zinc oxide ball milling, S3, mixed ball milling, S4, spray granulation, S5, pressure forming and S6, target material sintering. The preparation method comprises the following steps: selecting indium oxide, tin oxide and zinc oxide with specific BET values as raw materials, uniformly mixing the powder through stirring and ball milling, drying through a centrifugal spray granulator to obtain IZTO powder, compressing the IZTO powder into a green body by using an isostatic pressing forming machine, and sintering in a normal-pressure oxygen atmosphere to obtain the IZTO ceramic material. And the heating rate and the heat preservation time are controlled to prepare the high-density target material. Compared with the traditional process, the scheme can greatly improve the density and uniformity of the target material, and has remarkable application value.
一种高密度IZTO靶材的制备方法
本发明涉及靶材技术领域,具体涉及一种高密度IZTO靶材的制备方法,所述制备方法包括如下步骤:S1原材料选择、S2氧化锌球磨、S3混合球磨、S4喷雾造粒、S5压力成型、S6靶材烧结。本发明选用特定BET值的氧化铟、氧化锡和氧化锌作为原材料,通过搅拌球磨使粉末混合均匀,经离心式喷雾造粒机干燥造成IZTO粉末,再使用等静压成型机将IZTO粉末压缩成素胚,然后在常压氧气气氛下进行烧结处理,控制升温速率和保温时间以实现高密度靶材的制备。与传统工艺相比,该方案可大幅度提高靶材的密度和均匀性,具有显著的应用价值。
The invention relates to the technical field of target materials, in particular to a high-density IZTO target material preparation method which comprises the following steps: S1, raw material selection, S2, zinc oxide ball milling, S3, mixed ball milling, S4, spray granulation, S5, pressure forming and S6, target material sintering. The preparation method comprises the following steps: selecting indium oxide, tin oxide and zinc oxide with specific BET values as raw materials, uniformly mixing the powder through stirring and ball milling, drying through a centrifugal spray granulator to obtain IZTO powder, compressing the IZTO powder into a green body by using an isostatic pressing forming machine, and sintering in a normal-pressure oxygen atmosphere to obtain the IZTO ceramic material. And the heating rate and the heat preservation time are controlled to prepare the high-density target material. Compared with the traditional process, the scheme can greatly improve the density and uniformity of the target material, and has remarkable application value.
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