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Thermally-induced coagulation microcapsule for cement-based material and preparation method of thermally-induced coagulation microcapsule
The invention discloses a thermally-induced coagulation microcapsule for cement-based materials and a preparation method thereof.The preparation method of the thermally-induced coagulation microcapsule comprises the following steps that 1, paraffin solid and a solvent A are placed in a container according to a certain volume ratio, then heating is conducted at a certain temperature, paraffin is melted into a liquid state, the solvent A and the paraffin are not mutually fused, and the solvent A and the paraffin are not mutually fused; the boiling point of the polar organic compound is far higher than the melting point of paraffin; and 2) adding a coagulation accelerator into the molten liquid paraffin, uniformly stirring, cooling in an ice-water mixture, and then carrying out suction filtration to obtain the thermally induced coagulation microcapsule for the cement-based material. The particle size of the thermally-induced coagulation-accelerating microcapsule is 60-150 [mu] m, and when the thermally-induced coagulation-accelerating microcapsule is applied to a cement-based material, the early-stage fluidity of the cement-based cementing material can be ensured, and the coagulation time of the cement-based cementing material can be accurately controlled.
本发明公开了一种用于水泥基材料热致促凝微胶囊及其制备方法,该热致促凝微胶囊的制备方法,包括以下步骤:1)将石蜡固体与溶剂A按一定的体积比置于容器中,然后,于一定温度下加热,使石蜡融化为液态,其中,溶剂A为与石蜡互不相融,无味无挥发性,且沸点远远高于石蜡熔点的极性有机化合物;2)向融化的液态石蜡中加入促凝剂,搅拌均匀后,置于冰水混合物中冷却,然后,抽滤,得到用于水泥基材料热致促凝微胶囊。本发明所得的热致促凝微胶囊的粒径为60~150μm,当将其用于水泥基材料时既可以保证水泥基胶凝材料前期的流动性,又可以精准控制其凝结时间。
Thermally-induced coagulation microcapsule for cement-based material and preparation method of thermally-induced coagulation microcapsule
The invention discloses a thermally-induced coagulation microcapsule for cement-based materials and a preparation method thereof.The preparation method of the thermally-induced coagulation microcapsule comprises the following steps that 1, paraffin solid and a solvent A are placed in a container according to a certain volume ratio, then heating is conducted at a certain temperature, paraffin is melted into a liquid state, the solvent A and the paraffin are not mutually fused, and the solvent A and the paraffin are not mutually fused; the boiling point of the polar organic compound is far higher than the melting point of paraffin; and 2) adding a coagulation accelerator into the molten liquid paraffin, uniformly stirring, cooling in an ice-water mixture, and then carrying out suction filtration to obtain the thermally induced coagulation microcapsule for the cement-based material. The particle size of the thermally-induced coagulation-accelerating microcapsule is 60-150 [mu] m, and when the thermally-induced coagulation-accelerating microcapsule is applied to a cement-based material, the early-stage fluidity of the cement-based cementing material can be ensured, and the coagulation time of the cement-based cementing material can be accurately controlled.
本发明公开了一种用于水泥基材料热致促凝微胶囊及其制备方法,该热致促凝微胶囊的制备方法,包括以下步骤:1)将石蜡固体与溶剂A按一定的体积比置于容器中,然后,于一定温度下加热,使石蜡融化为液态,其中,溶剂A为与石蜡互不相融,无味无挥发性,且沸点远远高于石蜡熔点的极性有机化合物;2)向融化的液态石蜡中加入促凝剂,搅拌均匀后,置于冰水混合物中冷却,然后,抽滤,得到用于水泥基材料热致促凝微胶囊。本发明所得的热致促凝微胶囊的粒径为60~150μm,当将其用于水泥基材料时既可以保证水泥基胶凝材料前期的流动性,又可以精准控制其凝结时间。
Thermally-induced coagulation microcapsule for cement-based material and preparation method of thermally-induced coagulation microcapsule
一种用于水泥基材料热致促凝微胶囊及其制备方法
HUANG JIAN (Autor:in) / KUANG HAO (Autor:in) / HU HAILONG (Autor:in) / LYU RUOYUN (Autor:in) / HUANG JIYUN (Autor:in) / LYU YANG (Autor:in) / TAN HONGBO (Autor:in) / JIAN SHOUWEI (Autor:in) / LEE SANG-KOOK (Autor:in) / MA BAOGUO (Autor:in)
15.03.2024
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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