Eine Plattform für die Wissenschaft: Bauingenieurwesen, Architektur und Urbanistik
Eine Plattform für die Wissenschaft: Bauingenieurwesen, Architektur und Urbanistik
Method for synthesizing titanium diboride powder
The present invention relates to a method for preparing a TiB2 powder comprising reducing titanium oxide with carbon in the presence of a boron source, said method comprising heating a mixture of a carbon source, a boron carbide powder and a titanium oxide powder wherein the boron carbide powder has a median diameter of between 5 [mu] m and 100 [mu] m and the titanium oxide powder has a median diameter of between 5 [mu] m and 80 [mu] m, the mixture is placed in an enclosure at a temperature between 1500 DEG C and 2000 DEG C at an inert gas purge flow rate of 0.5-10 L/min/m/m3 of the enclosure; and a TiB2 powder obtained by such a method.
本发明涉及一种用于制备TiB2粉末的方法，包括在硼源存在下用碳还原氧化钛，所述方法包括加热碳源、碳化硼粉末和氧化钛粉末的混合物，其中碳化硼粉末的中值粒径在5μm和100μm之间，氧化钛粉末的中值粒径在5μm和80μm之间，所述混合物被放置在外壳中，在1500℃和2000℃之间的温度下，在0.5‑10L/min/m/m3外壳的惰性气体吹扫流速下；以及通过这种方法获得TiB2粉末。
Method for synthesizing titanium diboride powder
The present invention relates to a method for preparing a TiB2 powder comprising reducing titanium oxide with carbon in the presence of a boron source, said method comprising heating a mixture of a carbon source, a boron carbide powder and a titanium oxide powder wherein the boron carbide powder has a median diameter of between 5 [mu] m and 100 [mu] m and the titanium oxide powder has a median diameter of between 5 [mu] m and 80 [mu] m, the mixture is placed in an enclosure at a temperature between 1500 DEG C and 2000 DEG C at an inert gas purge flow rate of 0.5-10 L/min/m/m3 of the enclosure; and a TiB2 powder obtained by such a method.
本发明涉及一种用于制备TiB2粉末的方法，包括在硼源存在下用碳还原氧化钛，所述方法包括加热碳源、碳化硼粉末和氧化钛粉末的混合物，其中碳化硼粉末的中值粒径在5μm和100μm之间，氧化钛粉末的中值粒径在5μm和80μm之间，所述混合物被放置在外壳中，在1500℃和2000℃之间的温度下，在0.5‑10L/min/m/m3外壳的惰性气体吹扫流速下；以及通过这种方法获得TiB2粉末。
Method for synthesizing titanium diboride powder
用于合成二硼化钛粉末的方法
AFHAD MOHAMMAD REZA (Autor:in) / NONNET EMMANUEL (Autor:in) / SAN-MIGUEL LAURIE (Autor:in)
24.05.2024
Patent
Elektronische Ressource
Chinesisch
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