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Magnesia carbon brick with good thermal shock resistance stability and preparation method thereof
The invention relates to the technical field of refractory materials, and particularly discloses a magnesia carbon brick with good thermal shock resistance stability, which is prepared from the following raw materials in parts by mass: 30 to 100 parts of fused magnesia, 10 to 50 parts of carbon source, 1 to 5 parts of metal aluminum powder, 1 to 5 parts of calcium hexaluminate, 1 to 5 parts of phenolic resin, 1 to 5 parts of vanadium diboride, 1 to 5 parts of steel fiber and 1 to 2 parts of steel particle. The invention also discloses a preparation method of the magnesia carbon brick with good thermal shock resistance stability, which comprises the following steps: mixing the fused magnesia, the carbon source, the metal aluminum powder and the calcium hexaluminate, stirring at 30-40 DEG C for 10-30 minutes, adding the phenolic resin, and continuously stirring to obtain a premix a; adding vanadium diboride, steel fibers and steel particles into the premix a, uniformly mixing, and stirring at 1-10 DEG C for 5-15 minutes to obtain a premix b; aging the premix b for 1-2 hours, carrying out pressure forming, curing at 120-180 DEG C for 10-20 hours, and carrying out heat treatment at 1350-1420 DEG C for 1-2 hours.
本发明涉及耐火材料技术领域,具体公开了一种抗热震稳定性好的镁碳砖,其原料按质量份包括:电熔镁砂30‑100份,碳源10‑50份,金属铝粉1‑5份,六铝酸钙1‑5份,酚醛树脂1‑5份,二硼化钒1‑5份,钢纤维1‑5份,钢粒1‑2份。本发明还公开了上述抗热震稳定性好的镁碳砖制备方法,包括:将电熔镁砂、碳源、金属铝粉、六铝酸钙混合,30‑40℃搅拌10‑30min,加入酚醛树脂继续搅拌得到预混料a;向预混料a中加入二硼化钒、钢纤维、钢粒混合均匀,1‑10℃搅拌5‑15min,得到预混料b;将预混料b困料1‑2h,加压成型,120‑180℃固化10‑20h,1350‑1420℃热处理1‑2h。
Magnesia carbon brick with good thermal shock resistance stability and preparation method thereof
The invention relates to the technical field of refractory materials, and particularly discloses a magnesia carbon brick with good thermal shock resistance stability, which is prepared from the following raw materials in parts by mass: 30 to 100 parts of fused magnesia, 10 to 50 parts of carbon source, 1 to 5 parts of metal aluminum powder, 1 to 5 parts of calcium hexaluminate, 1 to 5 parts of phenolic resin, 1 to 5 parts of vanadium diboride, 1 to 5 parts of steel fiber and 1 to 2 parts of steel particle. The invention also discloses a preparation method of the magnesia carbon brick with good thermal shock resistance stability, which comprises the following steps: mixing the fused magnesia, the carbon source, the metal aluminum powder and the calcium hexaluminate, stirring at 30-40 DEG C for 10-30 minutes, adding the phenolic resin, and continuously stirring to obtain a premix a; adding vanadium diboride, steel fibers and steel particles into the premix a, uniformly mixing, and stirring at 1-10 DEG C for 5-15 minutes to obtain a premix b; aging the premix b for 1-2 hours, carrying out pressure forming, curing at 120-180 DEG C for 10-20 hours, and carrying out heat treatment at 1350-1420 DEG C for 1-2 hours.
本发明涉及耐火材料技术领域,具体公开了一种抗热震稳定性好的镁碳砖,其原料按质量份包括:电熔镁砂30‑100份,碳源10‑50份,金属铝粉1‑5份,六铝酸钙1‑5份,酚醛树脂1‑5份,二硼化钒1‑5份,钢纤维1‑5份,钢粒1‑2份。本发明还公开了上述抗热震稳定性好的镁碳砖制备方法,包括:将电熔镁砂、碳源、金属铝粉、六铝酸钙混合,30‑40℃搅拌10‑30min,加入酚醛树脂继续搅拌得到预混料a;向预混料a中加入二硼化钒、钢纤维、钢粒混合均匀,1‑10℃搅拌5‑15min,得到预混料b;将预混料b困料1‑2h,加压成型,120‑180℃固化10‑20h,1350‑1420℃热处理1‑2h。
Magnesia carbon brick with good thermal shock resistance stability and preparation method thereof
一种抗热震稳定性好的镁碳砖及其制备方法
ZHANG GUOHUA (Autor:in) / ZHUANG ZHIGANG (Autor:in) / ZHUANG HONGLIANG (Autor:in) / ZHUANG JUNYING (Autor:in)
16.08.2024
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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