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Preparation method of high-temperature-resistant hafnium boride ceramic material
The invention discloses a preparation method of a high-temperature-resistant hafnium boride ceramic material, and belongs to the technical field of ceramic materials, the preparation method comprises the following steps: preparing composite hafnium boride powder, preparing composite silicon carbide powder, mixing and sintering; the preparation of the composite hafnium boride powder comprises the following steps: preparing first-stage coated powder, preparing second-stage coated powder, preparing third-stage coated powder, and firing. The preparation of the composite silicon carbide powder comprises the following steps: primary treatment and secondary treatment; in the step of material mixing, composite hafnium boride powder, composite silicon carbide powder and absolute ethyl alcohol are mixed according to the mass ratio of (70-72): (28-30): (160-200), ball milling is conducted for 4-5 h, then drying is conducted, and mixed powder is obtained. The prepared high-temperature-resistant hafnium boride ceramic material is high in density and good in thermal stability, thermal shock resistance, mechanical property and heat-conducting property.
本发明公开了一种耐高温硼化铪陶瓷材料的制备方法,属于陶瓷材料技术领域,所述制备方法由以下步骤组成:制备复合硼化铪粉,制备复合碳化硅粉,混料,烧结;所述制备复合硼化铪粉,由以下步骤组成:制备一级包覆粉,制备二级包覆粉,制备三级包覆粉,烧制;所述制备复合碳化硅粉,由以下步骤组成:一级处理,二级处理;所述混料,将复合硼化铪粉、复合碳化硅粉、无水乙醇按照质量比为70‑72:28‑30:160‑200混合后,球磨4‑5h后烘干,得到混合粉。本发明制备的耐高温硼化铪陶瓷材料的致密度高,热稳定性能、抗热震性能、机械性能、导热性能好。
Preparation method of high-temperature-resistant hafnium boride ceramic material
The invention discloses a preparation method of a high-temperature-resistant hafnium boride ceramic material, and belongs to the technical field of ceramic materials, the preparation method comprises the following steps: preparing composite hafnium boride powder, preparing composite silicon carbide powder, mixing and sintering; the preparation of the composite hafnium boride powder comprises the following steps: preparing first-stage coated powder, preparing second-stage coated powder, preparing third-stage coated powder, and firing. The preparation of the composite silicon carbide powder comprises the following steps: primary treatment and secondary treatment; in the step of material mixing, composite hafnium boride powder, composite silicon carbide powder and absolute ethyl alcohol are mixed according to the mass ratio of (70-72): (28-30): (160-200), ball milling is conducted for 4-5 h, then drying is conducted, and mixed powder is obtained. The prepared high-temperature-resistant hafnium boride ceramic material is high in density and good in thermal stability, thermal shock resistance, mechanical property and heat-conducting property.
本发明公开了一种耐高温硼化铪陶瓷材料的制备方法,属于陶瓷材料技术领域,所述制备方法由以下步骤组成:制备复合硼化铪粉,制备复合碳化硅粉,混料,烧结;所述制备复合硼化铪粉,由以下步骤组成:制备一级包覆粉,制备二级包覆粉,制备三级包覆粉,烧制;所述制备复合碳化硅粉,由以下步骤组成:一级处理,二级处理;所述混料,将复合硼化铪粉、复合碳化硅粉、无水乙醇按照质量比为70‑72:28‑30:160‑200混合后,球磨4‑5h后烘干,得到混合粉。本发明制备的耐高温硼化铪陶瓷材料的致密度高,热稳定性能、抗热震性能、机械性能、导热性能好。
Preparation method of high-temperature-resistant hafnium boride ceramic material
一种耐高温硼化铪陶瓷材料的制备方法
WANG HAORAN (Autor:in) / LI HAN (Autor:in) / LIU YUN (Autor:in) / TIAN FANG (Autor:in) / YANG YANG (Autor:in) / LIU HONGHUA (Autor:in) / WANG MENGMENG (Autor:in) / LI ZHANFENG (Autor:in) / ZHANG PINGPING (Autor:in) / LIU JIA (Autor:in)
17.12.2024
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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