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Methods of preparing aerogels and aerogel slurries and aerogels and slurries prepared thereby
A method of preparing a silica or alumina wet gel for use in the preparation of an aerogel or aerogel slurry. The method comprises providing a precursor comprising an alkylsilane and/or a metal alkoxide, e.g. aluminium tri-sec-butoxide, and reacting the precursor in the presence of a sol-gel solvent and an alkaline earth metal oxide solid gelation agent to form a wet-gel. The oxide may be calcium oxide, magnesium oxide, strontium oxide or barium oxide. The wet gel may be blended to form a slurry mixture and a drying agent may be added. The method may further comprise introducing carbon dioxide gas to the wet-gel or slurry mixture to form an aerogel or aerogel slurry. A kit may comprise an alkylsilane and/or a metal alkoxide, an alkaline earth metal oxide solid, an alcohol, and instructions for performing the method.
Methods of preparing aerogels and aerogel slurries and aerogels and slurries prepared thereby
A method of preparing a silica or alumina wet gel for use in the preparation of an aerogel or aerogel slurry. The method comprises providing a precursor comprising an alkylsilane and/or a metal alkoxide, e.g. aluminium tri-sec-butoxide, and reacting the precursor in the presence of a sol-gel solvent and an alkaline earth metal oxide solid gelation agent to form a wet-gel. The oxide may be calcium oxide, magnesium oxide, strontium oxide or barium oxide. The wet gel may be blended to form a slurry mixture and a drying agent may be added. The method may further comprise introducing carbon dioxide gas to the wet-gel or slurry mixture to form an aerogel or aerogel slurry. A kit may comprise an alkylsilane and/or a metal alkoxide, an alkaline earth metal oxide solid, an alcohol, and instructions for performing the method.
Methods of preparing aerogels and aerogel slurries and aerogels and slurries prepared thereby
XIAO HAN (Autor:in) / NING ZHANG (Autor:in)
15.05.2024
Patent
Elektronische Ressource
Englisch
IPC:
C04B
Kalk
,
LIME
/
B01J
Chemische oder physikalische Verfahren, z.B. Katalyse oder Kolloidchemie
,
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
/
C01B
NON-METALLIC ELEMENTS
,
Nichtmetallische Elemente
/
C01F
COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
,
Verbindungen der Metalle Beryllium, Magnesium, Aluminium, Calcium, Strontium, Barium, Radium, Thorium oder der Seltenen Erden
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