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Synthesis of 3-alkyl(aryl)thietanes

Shevchenko, S. E. / Volynskii, N. P.

Abstract A preparative procedure for the synthesis of thietanes bearing alkyl substituents in the β-position was developed. Using this procedure, 3-substituted thietanes can be obtained in four steps with an ultimate yield of > 50%. 3-R-thietanes (where R = CH3, C4H9, C5H11, C6H13, C6H5) and the corresponding sulfoxides and sulfones were synthesized and examined. The feasibility of preparation of gem-3,3-substituted thietanes was exemplified by the synthesis of 3,3-dihexylthietane.

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Synthesis of 3-alkyl(aryl)thietanes

Shevchenko, S. E. / Volynskii, N. P.

Abstract A preparative procedure for the synthesis of thietanes bearing alkyl substituents in the β-position was developed. Using this procedure, 3-substituted thietanes can be obtained in four steps with an ultimate yield of > 50%. 3-R-thietanes (where R = CH3, C4H9, C5H11, C6H13, C6H5) and the corresponding sulfoxides and sulfones were synthesized and examined. The feasibility of preparation of gem-3,3-substituted thietanes was exemplified by the synthesis of 3,3-dihexylthietane.

Synthesis of 3-alkyl(aryl)thietanes

Shevchenko, S. E. / Volynskii, N. P.

Abstract A preparative procedure for the synthesis of thietanes bearing alkyl substituents in the β-position was developed. Using this procedure, 3-substituted thietanes can be obtained in four steps with an ultimate yield of > 50%. 3-R-thietanes (where R = CH3, C4H9, C5H11, C6H13, C6H5) and the corresponding sulfoxides and sulfones were synthesized and examined. The feasibility of preparation of gem-3,3-substituted thietanes was exemplified by the synthesis of 3,3-dihexylthietane.

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Titel:

Synthesis of 3-alkyl(aryl)thietanes

Beteiligte:

Shevchenko, S. E. (Autor:in) / Volynskii, N. P. (Autor:in)

Erschienen in:

Petroleum Chemistry ; 48 ; 123-128

Erscheinungsdatum:

01.03.2008

Format / Umfang:

6 pages

ISSN:

1555-6239 , 0965-5441

DOI:

https://doi.org/10.1134/S0965544108020084

Medientyp:

Aufsatz (Zeitschrift)

Format:

Elektronische Ressource

Sprache:

Englisch

Schlagwörter:

Propanediol , Petroleum Chemistry , Sulfonyl Chloride , Lithium Aluminum Hydride , Organic Sulfur Compound Chemistry , Industrial Chemistry/Chemical Engineering

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