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Pseudomorphic Transformation of Porous Glasses into Micelle‐Templated Silica

Uhlig, Hans / Hollenbach, Julia / Rogaczewski, Matthias / Matysik, Jörg / Brieler, Felix J. / Fröba, Michael / Enke, Dirk

Micelle‐templated silica (MTS)‐composites with flexible macroscopic shape, monomodal or bimodal (hierarchical) pore structure, and high mechanical stability can be prepared by partial or complete pseudomorphic transformation of porous glasses (PG). The state of research concerning synthesis, transformation mechanism, characterization, and application of MTS/PG‐composites is reviewed and the investigation of the transformation products by ¹²⁹Xe NMR spectroscopy and the direct synthesis of Al‐MCM‐41/PG‐composites are introduced. Finally, several approaches like a double‐templating strategy for pore protection is shown.

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Pseudomorphic Transformation of Porous Glasses into Micelle‐Templated Silica

Uhlig, Hans / Hollenbach, Julia / Rogaczewski, Matthias / Matysik, Jörg / Brieler, Felix J. / Fröba, Michael / Enke, Dirk

Micelle‐templated silica (MTS)‐composites with flexible macroscopic shape, monomodal or bimodal (hierarchical) pore structure, and high mechanical stability can be prepared by partial or complete pseudomorphic transformation of porous glasses (PG). The state of research concerning synthesis, transformation mechanism, characterization, and application of MTS/PG‐composites is reviewed and the investigation of the transformation products by ¹²⁹Xe NMR spectroscopy and the direct synthesis of Al‐MCM‐41/PG‐composites are introduced. Finally, several approaches like a double‐templating strategy for pore protection is shown.

Pseudomorphic Transformation of Porous Glasses into Micelle‐Templated Silica

Uhlig, Hans / Hollenbach, Julia / Rogaczewski, Matthias / Matysik, Jörg / Brieler, Felix J. / Fröba, Michael / Enke, Dirk

Micelle‐templated silica (MTS)‐composites with flexible macroscopic shape, monomodal or bimodal (hierarchical) pore structure, and high mechanical stability can be prepared by partial or complete pseudomorphic transformation of porous glasses (PG). The state of research concerning synthesis, transformation mechanism, characterization, and application of MTS/PG‐composites is reviewed and the investigation of the transformation products by ¹²⁹Xe NMR spectroscopy and the direct synthesis of Al‐MCM‐41/PG‐composites are introduced. Finally, several approaches like a double‐templating strategy for pore protection is shown.

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Titel:

Pseudomorphic Transformation of Porous Glasses into Micelle‐Templated Silica

Beteiligte:

Uhlig, Hans (Autor:in) / Hollenbach, Julia (Autor:in) / Rogaczewski, Matthias (Autor:in) / Matysik, Jörg (Autor:in) / Brieler, Felix J. (Autor:in) / Fröba, Michael (Autor:in) / Enke, Dirk (Autor:in)

Erschienen in:

Chemie Ingenieur Technik ; 89 ; 863-875

Erscheinungsdatum:

01.07.2017

Format / Umfang:

13 pages

ISSN:

0009-286X , 1522-2640

DOI:

https://doi.org/10.1002/cite.201600189

Medientyp:

Aufsatz (Zeitschrift)

Format:

Elektronische Ressource

Sprache:

Englisch

Schlagwörter:

NMR spectroscopy , Pseudomorphic transformation , Porous glasses , Silica composites

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