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Preparation method of self-healing silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material
The invention relates to a preparation method of a self-healing silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material, which comprises the following steps: (1) preparing a polyborosilazane (PBSZ) precursor; dissolving the PBSZ precursor in a toluene solution under the protection of N2 to obtain a PBSZ toluene solution; transferring into a pipe furnace, crosslinking under the protection of N2, grinding and screening to obtain SiBNC precursor powder; (2) preparing SiC fibers into a prefabricated part, carrying out hot pressing on the SiBNC precursor powder and SiC fiber prefabricated part, cooling and demolding to obtain a composite material; and transferring into a pipe furnace in an N2 protective atmosphere to perform ceramization, and finally, sintering. The method is simple in technique, easy to operate and low in cost; and the prepared silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material is uniform and compact, has the advantages of favorable high-temperature stability and excellent oxidation resistance, and especially has self-healing performance.
Preparation method of self-healing silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material
The invention relates to a preparation method of a self-healing silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material, which comprises the following steps: (1) preparing a polyborosilazane (PBSZ) precursor; dissolving the PBSZ precursor in a toluene solution under the protection of N2 to obtain a PBSZ toluene solution; transferring into a pipe furnace, crosslinking under the protection of N2, grinding and screening to obtain SiBNC precursor powder; (2) preparing SiC fibers into a prefabricated part, carrying out hot pressing on the SiBNC precursor powder and SiC fiber prefabricated part, cooling and demolding to obtain a composite material; and transferring into a pipe furnace in an N2 protective atmosphere to perform ceramization, and finally, sintering. The method is simple in technique, easy to operate and low in cost; and the prepared silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material is uniform and compact, has the advantages of favorable high-temperature stability and excellent oxidation resistance, and especially has self-healing performance.
Preparation method of self-healing silicon-carbide-fiber-reinforced silicon-boron-nitrogen-carbon composite material
YU MUHUO (author) / ZHANG CHENYU (author) / LIU YONG (author) / KE SHENGBAO (author)
2015-04-22
Patent
Electronic Resource
English
IPC:
C04B
Kalk
,
LIME
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