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Low temperature sinterable temperature stable ultralow dielectric constant microwave dielectric ceramic Li2Zn2YV3O12
The invention discloses a low temperature sinterable temperature stable ultralow dielectric constant microwave dielectric ceramic Li2Zn2YV3O12 and a preparation method thereof. The method includes: (1) weighing Li2CO3, ZnO, Y2O3 and V2O5 original powder with purity of over 99.9% (weight percentage) according to the composition of Li2Zn2YV3O12; (2) subjecting the raw materials of step (1) to wet ball-milling mixing for 12h, taking distilled water as the ball-milling medium, performing drying, then conducting presintering in 700DEG C air atmosphere for 6h; and (3) adding a binder into the powder prepared in step (2) and conducting granulation, then performing compression moulding, and finally conducting sintering in 750-800DEG C air atmosphere for 4h. The binder adopts a polyvinyl alcohol solution with a mass concentration of 5%, and the adding amount of polyvinyl alcohol accounts for 3% of the total mass of the powder. The ceramic prepared by the method provided by the invention can be well sintered below 800DEG C, and has a dielectric constant up to 17.1-17.7, a quality factor Qf value up to 114000-146000GHz and a small temperature coefficient of resonant frequency, thus having enormous application value in industry.
Low temperature sinterable temperature stable ultralow dielectric constant microwave dielectric ceramic Li2Zn2YV3O12
The invention discloses a low temperature sinterable temperature stable ultralow dielectric constant microwave dielectric ceramic Li2Zn2YV3O12 and a preparation method thereof. The method includes: (1) weighing Li2CO3, ZnO, Y2O3 and V2O5 original powder with purity of over 99.9% (weight percentage) according to the composition of Li2Zn2YV3O12; (2) subjecting the raw materials of step (1) to wet ball-milling mixing for 12h, taking distilled water as the ball-milling medium, performing drying, then conducting presintering in 700DEG C air atmosphere for 6h; and (3) adding a binder into the powder prepared in step (2) and conducting granulation, then performing compression moulding, and finally conducting sintering in 750-800DEG C air atmosphere for 4h. The binder adopts a polyvinyl alcohol solution with a mass concentration of 5%, and the adding amount of polyvinyl alcohol accounts for 3% of the total mass of the powder. The ceramic prepared by the method provided by the invention can be well sintered below 800DEG C, and has a dielectric constant up to 17.1-17.7, a quality factor Qf value up to 114000-146000GHz and a small temperature coefficient of resonant frequency, thus having enormous application value in industry.
Low temperature sinterable temperature stable ultralow dielectric constant microwave dielectric ceramic Li2Zn2YV3O12
FANG WEISHUANG (author) / CHEN JINWU (author) / TANG YING (author)
2016-01-13
Patent
Electronic Resource
English
IPC:
C04B
Kalk
,
LIME
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