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Carbide high-entropy ceramic fiber and preparation method thereof
The invention discloses a carbide high-entropy ceramic fiber and a preparation method. The high-entropy ceramic fiber comprises at least four of Ti, Zr, Hf, V, Nb, Ta, Mo and W elements, the carbide high-entropy ceramic fiber is in a single crystalline phase, and each element is uniformly distributed in a molecular level. The preparation method of the high-entropy ceramic fiber comprises the following steps: uniformly mixing a carbide high-entropy ceramic precursor containing a target metal element, a spinning aid and a solvent to prepare a precursor spinning solution, and carrying out spinning, degumming and high-temperature solid solution treatment to prepare the carbide high-entropy ceramic fiber.
本发明公开了一种碳化物高熵陶瓷纤维及制备方法，所述高熵陶瓷纤维包括Ti、Zr、Hf、V、Nb、Ta、Mo、W元素中的至少4种，所述碳化物高熵陶瓷纤维呈单一晶相，且其中各元素呈分子级的均匀分布。所述高熵陶瓷纤维的制备方法包括：将含有目标金属元素的碳化物高熵陶瓷前驱体、纺丝助剂和溶剂混合均匀制成前驱体纺丝溶液，再经过纺丝、排胶和高温固溶工序，制得所述碳化物高熵陶瓷纤维。
Carbide high-entropy ceramic fiber and preparation method thereof
The invention discloses a carbide high-entropy ceramic fiber and a preparation method. The high-entropy ceramic fiber comprises at least four of Ti, Zr, Hf, V, Nb, Ta, Mo and W elements, the carbide high-entropy ceramic fiber is in a single crystalline phase, and each element is uniformly distributed in a molecular level. The preparation method of the high-entropy ceramic fiber comprises the following steps: uniformly mixing a carbide high-entropy ceramic precursor containing a target metal element, a spinning aid and a solvent to prepare a precursor spinning solution, and carrying out spinning, degumming and high-temperature solid solution treatment to prepare the carbide high-entropy ceramic fiber.
本发明公开了一种碳化物高熵陶瓷纤维及制备方法，所述高熵陶瓷纤维包括Ti、Zr、Hf、V、Nb、Ta、Mo、W元素中的至少4种，所述碳化物高熵陶瓷纤维呈单一晶相，且其中各元素呈分子级的均匀分布。所述高熵陶瓷纤维的制备方法包括：将含有目标金属元素的碳化物高熵陶瓷前驱体、纺丝助剂和溶剂混合均匀制成前驱体纺丝溶液，再经过纺丝、排胶和高温固溶工序，制得所述碳化物高熵陶瓷纤维。
Carbide high-entropy ceramic fiber and preparation method thereof
一种碳化物高熵陶瓷纤维及制备方法
ZHAO TONG (author) / LI WEI (author) / YE LI (author) / CHEN FENGHUA (author) / SUN YANAN (author)
2020-08-28
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
/
C08G
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
,
Makromolekulare Verbindungen, anders erhalten als durch Reaktionen, an denen nur ungesättigte Kohlenstoff-Kohlenstoff-Bindungen beteiligt sind
/
D01F
Chemische Gesichtspunkte bei der Herstellung von produzierten Filamenten, Zwirnen, Fasern, Borsten oder Bändern
,
CHEMICAL FEATURES IN THE MANUFACTURE OF MAN-MADE FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
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