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Preparation method of high-performance potassium-sodium niobate-based lead-free energy storage ceramic
The invention belongs to the field of dielectric capacitor materials, and particularly relates to a preparation method of high-performance potassium-sodium niobate-based lead-free energy storage capacitor ceramic. The potassium-sodium niobate-based ceramic powder is obtained from industrial raw materials through a solid-phase method, a ceramic sample is obtained through unique two-stage sintering,and the energy storage density of the sample is obtained through ferroelectric hysteresis loop testing and calculation. Firstly, the ball milling time of ceramic powder and the two-stage sintering schedule of a green body are adjusted, and then the effective energy storage density and efficiency of the ceramic powder are obtained through ferroelectric analysis. The preparation method of the potassium-sodium niobate-based energy storage ceramic material is simple, convenient and capable of effectively obtaining high energy storage density and efficiency, and has reference significance for preparation of energy storage ceramic materials of other systems.
本发明属于电介质电容器材料领域,具体涉及一种高性能铌酸钾钠基无铅储能电容器陶瓷的制备方法。本发明的铌酸钾钠基陶瓷粉料采用工业原料经过固相法获得,陶瓷样品由独特的两段式烧结得到,样品的储能密度由电滞回线测试和计算得到。首先调节陶瓷粉料的球磨时间与生坯的两段式烧结制度,然后通过铁电分析得到其有效储能密度与效率。本发明实现了一种简便且有效获得高储能密度与效率的铌酸钾钠基储能陶瓷材料制备方法,对其他体系的储能陶瓷材料的制备具有借鉴意义。
Preparation method of high-performance potassium-sodium niobate-based lead-free energy storage ceramic
The invention belongs to the field of dielectric capacitor materials, and particularly relates to a preparation method of high-performance potassium-sodium niobate-based lead-free energy storage capacitor ceramic. The potassium-sodium niobate-based ceramic powder is obtained from industrial raw materials through a solid-phase method, a ceramic sample is obtained through unique two-stage sintering,and the energy storage density of the sample is obtained through ferroelectric hysteresis loop testing and calculation. Firstly, the ball milling time of ceramic powder and the two-stage sintering schedule of a green body are adjusted, and then the effective energy storage density and efficiency of the ceramic powder are obtained through ferroelectric analysis. The preparation method of the potassium-sodium niobate-based energy storage ceramic material is simple, convenient and capable of effectively obtaining high energy storage density and efficiency, and has reference significance for preparation of energy storage ceramic materials of other systems.
本发明属于电介质电容器材料领域,具体涉及一种高性能铌酸钾钠基无铅储能电容器陶瓷的制备方法。本发明的铌酸钾钠基陶瓷粉料采用工业原料经过固相法获得,陶瓷样品由独特的两段式烧结得到,样品的储能密度由电滞回线测试和计算得到。首先调节陶瓷粉料的球磨时间与生坯的两段式烧结制度,然后通过铁电分析得到其有效储能密度与效率。本发明实现了一种简便且有效获得高储能密度与效率的铌酸钾钠基储能陶瓷材料制备方法,对其他体系的储能陶瓷材料的制备具有借鉴意义。
Preparation method of high-performance potassium-sodium niobate-based lead-free energy storage ceramic
一种高性能铌酸钾钠基无铅储能陶瓷的制备方法
HUAN YU (author) / WANG XIAOZHI (author) / WEI TAO (author)
2021-01-26
Patent
Electronic Resource
Chinese
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