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A platform for research: civil engineering, architecture and urbanism
Preparation method of zirconia ceramic 3D printing material
The invention provides a preparation method of a zirconium oxide ceramic 3D printing material. The method comprises the following steps: preparing an ammonium zirconium carbonate solution, preparing zirconium oxide ultrafine powder, adding a cross-linked polymer, a dispersing agent and deionized water into the zirconium oxide ultrafine powder,carrying out mixing and ball milling to obtain slurry,and adding carbon fibers and an adhesive into the slurry to obtain the zirconium oxide ceramic 3D printing material. The zirconium oxide ceramic 3D printing material is obtained through steps of preparing the ammonium zirconium carbonate solution and preparing the zirconium oxide ultrafine powder and the like, adding the cross-linked polymer, the dispersing agent and the deionized water into the obtained zirconium oxide ultrafine powder, carrying out mixing and ball milling to obtain slurry, and adding carbon fibers and the adhesive into the slurry. The preparation method has the advantages that the preparation method can be applied to 3D printing, cracks on the surface of the printed zirconia ceramic are few, meanwhile, the printed product is high in strength due to the fact that carbon fibers and adhesives are added into the material, and the preparation method is easy in raw material obtaining, simple in operation and low in production cost.
本发明提供了一种用于氧化锆陶瓷3D打印材料的制备方法，包括制备碳酸锆铵溶液、制备氧化锆超细粉体，在氧化锆超细粉体中加入交联体、分散剂和去离子水，混合球磨，得到浆料，再在浆料中加入碳纤维和粘接剂，得氧化锆陶瓷3D打印材料本发明通过制备碳酸锆铵溶液以及制备氧化锆超细粉体等各步骤的操作，最后得到氧化锆超细粉体，加入交联体、分散剂和去离子水，混合球磨，得到浆料，再在浆料中加入碳纤维和粘接剂，得氧化锆陶瓷3D打印材料，可以应用于3D打印，打印的氧化锆陶瓷表面的裂纹少，同时由于材料中添加了碳纤维和粘接剂，打印出的产品强度高，同时本申请的制备方法原料易得、操作简单、生产成本较低。
Preparation method of zirconia ceramic 3D printing material
The invention provides a preparation method of a zirconium oxide ceramic 3D printing material. The method comprises the following steps: preparing an ammonium zirconium carbonate solution, preparing zirconium oxide ultrafine powder, adding a cross-linked polymer, a dispersing agent and deionized water into the zirconium oxide ultrafine powder,carrying out mixing and ball milling to obtain slurry,and adding carbon fibers and an adhesive into the slurry to obtain the zirconium oxide ceramic 3D printing material. The zirconium oxide ceramic 3D printing material is obtained through steps of preparing the ammonium zirconium carbonate solution and preparing the zirconium oxide ultrafine powder and the like, adding the cross-linked polymer, the dispersing agent and the deionized water into the obtained zirconium oxide ultrafine powder, carrying out mixing and ball milling to obtain slurry, and adding carbon fibers and the adhesive into the slurry. The preparation method has the advantages that the preparation method can be applied to 3D printing, cracks on the surface of the printed zirconia ceramic are few, meanwhile, the printed product is high in strength due to the fact that carbon fibers and adhesives are added into the material, and the preparation method is easy in raw material obtaining, simple in operation and low in production cost.
本发明提供了一种用于氧化锆陶瓷3D打印材料的制备方法，包括制备碳酸锆铵溶液、制备氧化锆超细粉体，在氧化锆超细粉体中加入交联体、分散剂和去离子水，混合球磨，得到浆料，再在浆料中加入碳纤维和粘接剂，得氧化锆陶瓷3D打印材料本发明通过制备碳酸锆铵溶液以及制备氧化锆超细粉体等各步骤的操作，最后得到氧化锆超细粉体，加入交联体、分散剂和去离子水，混合球磨，得到浆料，再在浆料中加入碳纤维和粘接剂，得氧化锆陶瓷3D打印材料，可以应用于3D打印，打印的氧化锆陶瓷表面的裂纹少，同时由于材料中添加了碳纤维和粘接剂，打印出的产品强度高，同时本申请的制备方法原料易得、操作简单、生产成本较低。
Preparation method of zirconia ceramic 3D printing material
一种用于氧化锆陶瓷3D打印材料的制备方法
LIU WEI (author) / GAO CHANGQING (author)
2021-02-19
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
/
B33Y
ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
,
Additive (generative) Fertigung, d. h. die Herstellung von dreidimensionalen [3D] Bauteilen durch additive Abscheidung, additive Agglomeration oder additive Schichtung, z. B. durch 3D- Drucken, Stereolithografie oder selektives Lasersintern
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