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High-density quartz-zirconium oxide composite ceramic and preparation method thereof
The invention discloses high-density quartz-zirconium oxide compositeceramic and a preparation method thereof. The composite ceramic is mainly composed of a quartz phase, a zirconium oxide phase, a zirconite phase and a glass phase. In the high-density quartz-zirconium oxide composite ceramic, the content of the quartz phase is 4.7 to 67.1 wt%, the content of the zirconium oxide phase is 6.5 to 60.5 wt%, the content of the zirconite phase is 5.0 to 63.2 wt%, and the content of the glass phase is 15.1 to 28.3 wt%. The preparation method comprises the following steps: mixing aeolian sand and zirconium oxide, and carrying out ball milling to obtain a mixed raw material; drying and crushing the mixed raw materials; carrying out compression molding on the crushed mixed raw materials to obtain a composite ceramic green body; and sintering the composite ceramic green body to obtain the high-density quartz-zirconium oxide composite ceramic. According to the invention, the content of quartz, zirconium oxide, zirconite and glass phase in the ceramic is adjusted by adjusting the addition amount of zirconium oxide, the sintering temperature and the heat preservation time, so that the composite ceramic with different mechanical properties is obtained, and the series of ceramics meet the application requirements of various occasions (cost and performance).
本发明公开高致密度石英‑氧化锆复相陶瓷及其制备方法,复相陶瓷主要由石英相、氧化锆相、锆英石相和玻璃相组成;在所述高致密度石英‑氧化锆复相陶瓷中:所述石英相的含量为4.7‑67.1wt%,所述氧化锆相的含量为6.5‑60.5wt%,所述锆英石相的含量为5.0‑63.2wt%;所述玻璃相的含量为15.1‑28.3wt%;其制备方法包括如下步骤:将风积沙和氧化锆混合后球磨,得到混合原料;将混合原料干燥后粉碎;将粉碎后的混合原料压制成型,得到复相陶瓷坯体;复相陶瓷坯体烧结后即制备得到高致密度石英‑氧化锆复相陶瓷。本发明通过调节氧化锆的添加量、烧结温度和保温时间,调节陶瓷中石英、氧化锆、锆英石以及玻璃相含量,得到不同力学性能的复相陶瓷,这种系列化的陶瓷适应多种场合(成本、性能)的应用要求。
High-density quartz-zirconium oxide composite ceramic and preparation method thereof
The invention discloses high-density quartz-zirconium oxide compositeceramic and a preparation method thereof. The composite ceramic is mainly composed of a quartz phase, a zirconium oxide phase, a zirconite phase and a glass phase. In the high-density quartz-zirconium oxide composite ceramic, the content of the quartz phase is 4.7 to 67.1 wt%, the content of the zirconium oxide phase is 6.5 to 60.5 wt%, the content of the zirconite phase is 5.0 to 63.2 wt%, and the content of the glass phase is 15.1 to 28.3 wt%. The preparation method comprises the following steps: mixing aeolian sand and zirconium oxide, and carrying out ball milling to obtain a mixed raw material; drying and crushing the mixed raw materials; carrying out compression molding on the crushed mixed raw materials to obtain a composite ceramic green body; and sintering the composite ceramic green body to obtain the high-density quartz-zirconium oxide composite ceramic. According to the invention, the content of quartz, zirconium oxide, zirconite and glass phase in the ceramic is adjusted by adjusting the addition amount of zirconium oxide, the sintering temperature and the heat preservation time, so that the composite ceramic with different mechanical properties is obtained, and the series of ceramics meet the application requirements of various occasions (cost and performance).
本发明公开高致密度石英‑氧化锆复相陶瓷及其制备方法,复相陶瓷主要由石英相、氧化锆相、锆英石相和玻璃相组成;在所述高致密度石英‑氧化锆复相陶瓷中:所述石英相的含量为4.7‑67.1wt%,所述氧化锆相的含量为6.5‑60.5wt%,所述锆英石相的含量为5.0‑63.2wt%;所述玻璃相的含量为15.1‑28.3wt%;其制备方法包括如下步骤:将风积沙和氧化锆混合后球磨,得到混合原料;将混合原料干燥后粉碎;将粉碎后的混合原料压制成型,得到复相陶瓷坯体;复相陶瓷坯体烧结后即制备得到高致密度石英‑氧化锆复相陶瓷。本发明通过调节氧化锆的添加量、烧结温度和保温时间,调节陶瓷中石英、氧化锆、锆英石以及玻璃相含量,得到不同力学性能的复相陶瓷,这种系列化的陶瓷适应多种场合(成本、性能)的应用要求。
High-density quartz-zirconium oxide composite ceramic and preparation method thereof
高致密度石英-氧化锆复相陶瓷及其制备方法
SHI ZHIMING (author) / ZHANG YONG (author) / YAN HUA (author) / WANG WENBIN (author) / LUO HONGWEI (author)
2021-08-27
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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