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Method for preparing porous SiOC-based ceramic membrane support by combining laser 3D printing with impregnation cracking process
The invention relates to a method for preparing a porous SiOC-based ceramic membrane support by combining laser 3D printing with an impregnation cracking process, which comprises the following steps: (1) mixing polysiloxane PSO powder, SiC powder and phenolic resin to obtain mixed powder; (2) carrying out printing molding on the obtained mixed powder by using a laser 3D printer to obtain a green body; and (3) placing the obtained green body in liquid PSO, vacuumizing and dipping, placing in an inert atmosphere, and sintering at 1200-1400 DEG C to obtain the porous SiOC-based ceramic membrane support.
本发明涉及一种激光3D打印结合浸渍裂解工艺制备多孔SiOC基陶瓷膜支撑体的方法,包括:(1)将聚硅氧烷PSO粉体、SiC粉体和酚醛树脂混合,得到混合粉体;(2)所得的混合粉体使用激光3D打印机打印成型,得到坯体;(3)将所得坯体置于液态PSO中抽真空浸渍后置于惰性气氛中,在1200~1400℃下烧结,得到所述多孔SiOC基陶瓷膜支撑体。
Method for preparing porous SiOC-based ceramic membrane support by combining laser 3D printing with impregnation cracking process
The invention relates to a method for preparing a porous SiOC-based ceramic membrane support by combining laser 3D printing with an impregnation cracking process, which comprises the following steps: (1) mixing polysiloxane PSO powder, SiC powder and phenolic resin to obtain mixed powder; (2) carrying out printing molding on the obtained mixed powder by using a laser 3D printer to obtain a green body; and (3) placing the obtained green body in liquid PSO, vacuumizing and dipping, placing in an inert atmosphere, and sintering at 1200-1400 DEG C to obtain the porous SiOC-based ceramic membrane support.
本发明涉及一种激光3D打印结合浸渍裂解工艺制备多孔SiOC基陶瓷膜支撑体的方法,包括:(1)将聚硅氧烷PSO粉体、SiC粉体和酚醛树脂混合,得到混合粉体;(2)所得的混合粉体使用激光3D打印机打印成型,得到坯体;(3)将所得坯体置于液态PSO中抽真空浸渍后置于惰性气氛中,在1200~1400℃下烧结,得到所述多孔SiOC基陶瓷膜支撑体。
Method for preparing porous SiOC-based ceramic membrane support by combining laser 3D printing with impregnation cracking process
一种激光3D打印结合浸渍裂解工艺制备多孔SiOC基陶瓷膜支撑体的方法
YIN JIE (author) / WANG KANGLONG (author) / LIU XUEJIAN (author) / HUANG ZHENGREN (author) / CHEN ZHONGMING (author) / YAO XIUMIN (author) / SUN ANLE (author) / JIANG JINDI (author)
2023-03-31
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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