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Preparation method of liquid coal-saving environment-friendly raw material grinding aid
The invention discloses a preparation method of a liquid coal-saving environment-friendly raw material grinding aid, which is characterized in that triethanolamine, citric acid, aconitic acid and ceric ammonium sulfate are adopted, nitrogen protection is carried out, the temperature is kept at 90 +/-2 DEG C, and viscous liquid, namely, aconitic acid triethanolamine ester, is obtained; then, respectively adding ferric nitrate and lanthanum nitrate into a reactor, and adding pentaerythritol to obtain a solution A; and 3, adding 48-52% of the solution A and 30-36% of triethanolamine aconitate, uniformly mixing, adding 10-14% of calcium nitrate and 4-8% of sodium chloride, stirring and dissolving, and adjusting the pH value to 4.5-6.5 by using acid to obtain yellow liquid, namely the coal-saving environment-friendly raw material grinding aid. The adding amount of the coal-saving environment-friendly raw material grinding aid is about three ten thousandths of the mass of the raw material, so that the machine-hour yield of cement raw material grinding can be improved, the power consumption is reduced, the fineness is uniform, agglomeration is avoided, and the standard coal consumption of clinker sintering is reduced by 3-5%.
本发明公开了一种液体节煤环保型生料助磨剂的制备方法,其特征在于,采用三乙醇胺、柠檬酸、乌头酸、硫酸铈铵,氮气保护,于90±2℃恒温,得粘稠状液为乌头酸三乙醇胺酯;然后,在反应器中,分别加入硝酸铁,硝酸镧,加入季戊四醇,即得A液;第三步加入,A液:48~52%,乌头酸三乙醇胺酯:30~36%,混合均匀,加入硝酸钙:10~14%,氯化钠:4~8%,搅拌溶解,用酸调节pH在4.5~6.5之间,即得黄色液体为节煤环保型生料助磨剂。加入该节煤环保型生料助磨剂的量为生料质量的万分之三左右,可提高水泥生料粉磨台时产量,降低电耗,细度均匀,不团聚,降低熟料烧成标准煤耗3~5%之间。
Preparation method of liquid coal-saving environment-friendly raw material grinding aid
The invention discloses a preparation method of a liquid coal-saving environment-friendly raw material grinding aid, which is characterized in that triethanolamine, citric acid, aconitic acid and ceric ammonium sulfate are adopted, nitrogen protection is carried out, the temperature is kept at 90 +/-2 DEG C, and viscous liquid, namely, aconitic acid triethanolamine ester, is obtained; then, respectively adding ferric nitrate and lanthanum nitrate into a reactor, and adding pentaerythritol to obtain a solution A; and 3, adding 48-52% of the solution A and 30-36% of triethanolamine aconitate, uniformly mixing, adding 10-14% of calcium nitrate and 4-8% of sodium chloride, stirring and dissolving, and adjusting the pH value to 4.5-6.5 by using acid to obtain yellow liquid, namely the coal-saving environment-friendly raw material grinding aid. The adding amount of the coal-saving environment-friendly raw material grinding aid is about three ten thousandths of the mass of the raw material, so that the machine-hour yield of cement raw material grinding can be improved, the power consumption is reduced, the fineness is uniform, agglomeration is avoided, and the standard coal consumption of clinker sintering is reduced by 3-5%.
本发明公开了一种液体节煤环保型生料助磨剂的制备方法,其特征在于,采用三乙醇胺、柠檬酸、乌头酸、硫酸铈铵,氮气保护,于90±2℃恒温,得粘稠状液为乌头酸三乙醇胺酯;然后,在反应器中,分别加入硝酸铁,硝酸镧,加入季戊四醇,即得A液;第三步加入,A液:48~52%,乌头酸三乙醇胺酯:30~36%,混合均匀,加入硝酸钙:10~14%,氯化钠:4~8%,搅拌溶解,用酸调节pH在4.5~6.5之间,即得黄色液体为节煤环保型生料助磨剂。加入该节煤环保型生料助磨剂的量为生料质量的万分之三左右,可提高水泥生料粉磨台时产量,降低电耗,细度均匀,不团聚,降低熟料烧成标准煤耗3~5%之间。
Preparation method of liquid coal-saving environment-friendly raw material grinding aid
一种液体节煤环保型生料助磨剂的制备方法
LI HUIZHI (author) / WANG BAOQUAN (author)
2023-08-08
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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