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Preparation method of high-performance ZrB2-SiC ultrahigh-temperature ceramic for aerospace
The invention discloses a preparation method of high-performance ZrB2-SiC ultra-high-temperature ceramic for aerospace, which comprises the following steps: firstly, coating the surface of SiC powder with atomic state W by using hexacarbonyl W and a chemical vapor deposition method, and then mixing the atomic state W coated SiC powder and ZrB2 powder by using an electromagnetic stirring method to obtain ultra-high-temperature ceramic powder, and finally, the compact preparation of the ZrB2-SiC ultra-high-temperature ceramic is realized by adopting an SPS technology. The ZrB2-SiC ultrahigh-temperature ceramic prepared by the method has the structural characteristics of high compactness and fine grains, has high fracture toughness and excellent high-temperature oxidation resistance, and has a wide application prospect in the field of aerospace.
本发明公开了一种航空航天用高性能ZrB2‑SiC超高温陶瓷的制备方法,首先采用六羰基W和化学气相沉积法在SiC粉末表面包覆原子态W,然后利用电磁搅拌法将原子态W包覆SiC粉和ZrB2粉混合得到超高温陶瓷粉末,最后采用SPS技术实现ZrB2‑SiC超高温陶瓷的致密化制备。本发明所制备的ZrB2‑SiC超高温陶瓷,具有兼顾高致密性和细小晶粒的结构特征,具有高的断裂韧性和优异的高温抗氧化性能,在航空航天领域具有广泛的应用前景。
Preparation method of high-performance ZrB2-SiC ultrahigh-temperature ceramic for aerospace
The invention discloses a preparation method of high-performance ZrB2-SiC ultra-high-temperature ceramic for aerospace, which comprises the following steps: firstly, coating the surface of SiC powder with atomic state W by using hexacarbonyl W and a chemical vapor deposition method, and then mixing the atomic state W coated SiC powder and ZrB2 powder by using an electromagnetic stirring method to obtain ultra-high-temperature ceramic powder, and finally, the compact preparation of the ZrB2-SiC ultra-high-temperature ceramic is realized by adopting an SPS technology. The ZrB2-SiC ultrahigh-temperature ceramic prepared by the method has the structural characteristics of high compactness and fine grains, has high fracture toughness and excellent high-temperature oxidation resistance, and has a wide application prospect in the field of aerospace.
本发明公开了一种航空航天用高性能ZrB2‑SiC超高温陶瓷的制备方法,首先采用六羰基W和化学气相沉积法在SiC粉末表面包覆原子态W,然后利用电磁搅拌法将原子态W包覆SiC粉和ZrB2粉混合得到超高温陶瓷粉末,最后采用SPS技术实现ZrB2‑SiC超高温陶瓷的致密化制备。本发明所制备的ZrB2‑SiC超高温陶瓷,具有兼顾高致密性和细小晶粒的结构特征,具有高的断裂韧性和优异的高温抗氧化性能,在航空航天领域具有广泛的应用前景。
Preparation method of high-performance ZrB2-SiC ultrahigh-temperature ceramic for aerospace
一种航空航天用高性能ZrB2-SiC超高温陶瓷的制备方法
YU YUAN (author) / QIAO ZHUHUI (author) / LIU WEIMIN (author) / HU BIN (author) / ZHANG XIAOFAN (author) / LI TONGYANG (author) / WANG LUJIE (author) / TANG HUAGUO (author)
2024-01-19
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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