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A platform for research: civil engineering, architecture and urbanism
Preparation method of ultra-high-temperature-resistant spin-coated glass film layer
The invention relates to a preparation method of an ultrahigh-temperature-resistant spin-coating glass film layer, which comprises the following steps of: S1, continuously spin-coating a spin-coating glass material on a substrate for three times at the spin-coating rate of 350rpm/min; s2, baking at the temperature of 200 DEG C for 60 seconds after the third spin coating, and cooling for 20 minutes after baking; s3, carrying out spin coating for the fourth time and the fifth time, wherein the spin coating rate is 350rpm/min; and after the fifth spin coating is finished, baking at the temperature of 200 DEG C for 60 seconds, and cooling for 20 minutes after baking to obtain the ultra-high-temperature-resistant spin-coated glass film layer. According to the preparation method of the ultra-high-temperature-resistant spin-coated glass film layer, the ultra-high-temperature-resistant spin-coated glass film layer has ultra-high-temperature resistance, and a 0.9-1 micron intact film layer can still be reserved at the high temperature of 950-1100 DEG C.
本发明涉及耐超高温旋涂玻璃膜层制备方法，S1、将旋涂玻璃材料在基体上连续旋涂三次，旋涂速率为350rpm/mi n；S2、第三次旋涂后在200℃温度下烘烤60秒，烘烤后冷却20分钟；S3、进行第四次和第五次旋涂，旋涂速率为350rpm/mi n；第五次旋涂结束后，在200℃温度下烘烤60秒，烘烤后冷却20分钟，获得耐超高温旋涂玻璃膜层。本发明的耐超高温旋涂玻璃膜层制备方法，具有耐超高温性能，在950‑1100℃高温，仍会保留0.9‑1微米完好膜层。
Preparation method of ultra-high-temperature-resistant spin-coated glass film layer
The invention relates to a preparation method of an ultrahigh-temperature-resistant spin-coating glass film layer, which comprises the following steps of: S1, continuously spin-coating a spin-coating glass material on a substrate for three times at the spin-coating rate of 350rpm/min; s2, baking at the temperature of 200 DEG C for 60 seconds after the third spin coating, and cooling for 20 minutes after baking; s3, carrying out spin coating for the fourth time and the fifth time, wherein the spin coating rate is 350rpm/min; and after the fifth spin coating is finished, baking at the temperature of 200 DEG C for 60 seconds, and cooling for 20 minutes after baking to obtain the ultra-high-temperature-resistant spin-coated glass film layer. According to the preparation method of the ultra-high-temperature-resistant spin-coated glass film layer, the ultra-high-temperature-resistant spin-coated glass film layer has ultra-high-temperature resistance, and a 0.9-1 micron intact film layer can still be reserved at the high temperature of 950-1100 DEG C.
本发明涉及耐超高温旋涂玻璃膜层制备方法，S1、将旋涂玻璃材料在基体上连续旋涂三次，旋涂速率为350rpm/mi n；S2、第三次旋涂后在200℃温度下烘烤60秒，烘烤后冷却20分钟；S3、进行第四次和第五次旋涂，旋涂速率为350rpm/mi n；第五次旋涂结束后，在200℃温度下烘烤60秒，烘烤后冷却20分钟，获得耐超高温旋涂玻璃膜层。本发明的耐超高温旋涂玻璃膜层制备方法，具有耐超高温性能，在950‑1100℃高温，仍会保留0.9‑1微米完好膜层。
Preparation method of ultra-high-temperature-resistant spin-coated glass film layer
一种耐超高温旋涂玻璃膜层制备方法
LI ZHENG (author) / WANG YUN (author) / YU LEI (author) / DUAN YIFEI (author) / LIU XIN (author) / HE DANDAN (author) / HUANG SHIQIAO (author) / GAN LIUHUA (author) / CHEN WEISHU (author) / CHEN ZIMING (author)
2024-01-26
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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