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Aluminum-silicon-yttrium ternary aerogel composite material and preparation method thereof
The invention discloses a preparation method of an aluminum-silicon-yttrium ternary aerogel composite material and the aluminum-silicon-yttrium ternary aerogel composite material prepared by the method. The preparation method of the aluminum-silicon-yttrium ternary aerogel composite material comprises the following steps: carrying out sol impregnation on a support body to obtain an impregnated support body; wherein the sol comprises silica sol and aluminum-yttrium sol; carrying out gelation treatment on the impregnated support body, so as to obtain a composite aluminum-yttrium-silica gel support body; and the composite aluminum-yttrium-silica gel supporting body is aged and dried, and the aluminum-silicon-yttrium ternary aerogel composite material is obtained. The prepared aluminum-silicon-yttrium ternary aerogel composite material has high-temperature stability, the heat conductivity at the temperature of 1200 DEG C is smaller than or equal to 0.105 W/m.k, and the volume shrinkage rate after heat treatment at the temperature of 1200 DEG C for 30 min is 4%-8% of the original volume.
本发明公开了一种铝‑硅‑钇三元气凝胶复合材料的制备方法以及所述方法制备得到的铝‑硅‑钇三元气凝胶复合材料;铝‑硅‑钇三元气凝胶复合材料的制备方法包括以下步骤:对支撑体进行溶胶浸渍,得到浸渍后的支撑体;其中,所述溶胶包括硅溶胶和铝‑钇溶胶;对浸渍后的所述支撑体进行凝胶化处理,得到复合铝‑钇‑硅凝胶支撑体;将所述复合铝‑钇‑硅凝胶支撑体进行老化、干燥,得到所述铝‑硅‑钇三元气凝胶复合材料。实现制得的铝‑硅‑钇三元气凝胶复合材料具有高温稳定性,在1200℃的热导率≤0.105W/m·k,1200℃热处理30min后体积收缩率为原体积的4‑8%。
Aluminum-silicon-yttrium ternary aerogel composite material and preparation method thereof
The invention discloses a preparation method of an aluminum-silicon-yttrium ternary aerogel composite material and the aluminum-silicon-yttrium ternary aerogel composite material prepared by the method. The preparation method of the aluminum-silicon-yttrium ternary aerogel composite material comprises the following steps: carrying out sol impregnation on a support body to obtain an impregnated support body; wherein the sol comprises silica sol and aluminum-yttrium sol; carrying out gelation treatment on the impregnated support body, so as to obtain a composite aluminum-yttrium-silica gel support body; and the composite aluminum-yttrium-silica gel supporting body is aged and dried, and the aluminum-silicon-yttrium ternary aerogel composite material is obtained. The prepared aluminum-silicon-yttrium ternary aerogel composite material has high-temperature stability, the heat conductivity at the temperature of 1200 DEG C is smaller than or equal to 0.105 W/m.k, and the volume shrinkage rate after heat treatment at the temperature of 1200 DEG C for 30 min is 4%-8% of the original volume.
本发明公开了一种铝‑硅‑钇三元气凝胶复合材料的制备方法以及所述方法制备得到的铝‑硅‑钇三元气凝胶复合材料;铝‑硅‑钇三元气凝胶复合材料的制备方法包括以下步骤:对支撑体进行溶胶浸渍,得到浸渍后的支撑体;其中,所述溶胶包括硅溶胶和铝‑钇溶胶;对浸渍后的所述支撑体进行凝胶化处理,得到复合铝‑钇‑硅凝胶支撑体;将所述复合铝‑钇‑硅凝胶支撑体进行老化、干燥,得到所述铝‑硅‑钇三元气凝胶复合材料。实现制得的铝‑硅‑钇三元气凝胶复合材料具有高温稳定性,在1200℃的热导率≤0.105W/m·k,1200℃热处理30min后体积收缩率为原体积的4‑8%。
Aluminum-silicon-yttrium ternary aerogel composite material and preparation method thereof
一种铝-硅-钇三元气凝胶复合材料及其制备方法
SUI XUEYE (author) / XU JIE (author) / LI ZHANFENG (author) / TANG WENZHE (author) / WANG MENGMENG (author) / DUAN XIAOFENG (author) / ZHOU CHANGLING (author) / LIU RUIXIANG (author)
2024-02-23
Patent
Electronic Resource
Chinese
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