A platform for research: civil engineering, architecture and urbanism
A platform for research: civil engineering, architecture and urbanism
Hydrophobic and oleophobic liquid hardening agent and preparation method thereof
The invention belongs to the technical field of building construction materials, and discloses a hydrophobic and oleophobic liquid hardening agent and a preparation method thereof. The preparation method comprises the following steps: at 40-70 DEG C, adding an active silicon powder aqueous solution into an organic-inorganic composite alkali aqueous solution, and stirring for reaction; filtering to obtain colorless transparent liquid A; adding an alcohol substance into the fluoroalkyl acrylate copolymer in a first stirring state, and controlling the pH value to be 7-9; adding a silane coupling agent into the obtained solution while stirring to obtain a mixed solution B; adding potassium methyl silicate into the colorless transparent liquid A at room temperature in a second stirring state, and stirring for reaction; then, adding a lithium silicate solution, and stirring for reaction; and finally, adding the mixed solution B, stirring and reacting until the solution is in a transparent state, thereby obtaining the hydrophobic and oleophobic liquid hardener. The product prepared by the preparation method disclosed by the invention has a relatively good anti-permeability effect.
本发明属于建筑施工材料技术领域，公开了一种疏水疏油型液体硬化剂及其制备方法；其中，所述制备方法包括：在40℃～70℃下，将活性硅粉水溶液加入到有机无机复合碱的水溶液，搅拌反应；过滤，得到无色透明液体A；在第一搅拌状态下，将醇类物质加入氟烷基丙烯酸酯共聚物，并控制pH值为7～9；在得到的溶液中边搅拌边加入硅烷偶联剂，得到混合溶液B；室温下，在第二搅拌状态下，将甲基硅酸钾加入所述无色透明液体A中，搅拌反应；然后，加入硅酸锂溶液，搅拌反应；最后，加入所述混合溶液B，搅拌反应直到溶液为透明状态，得到疏水疏油型液体硬化剂。本发明公开的制备方法制备获得的产品，具有较好的抗渗油效果。
Hydrophobic and oleophobic liquid hardening agent and preparation method thereof
The invention belongs to the technical field of building construction materials, and discloses a hydrophobic and oleophobic liquid hardening agent and a preparation method thereof. The preparation method comprises the following steps: at 40-70 DEG C, adding an active silicon powder aqueous solution into an organic-inorganic composite alkali aqueous solution, and stirring for reaction; filtering to obtain colorless transparent liquid A; adding an alcohol substance into the fluoroalkyl acrylate copolymer in a first stirring state, and controlling the pH value to be 7-9; adding a silane coupling agent into the obtained solution while stirring to obtain a mixed solution B; adding potassium methyl silicate into the colorless transparent liquid A at room temperature in a second stirring state, and stirring for reaction; then, adding a lithium silicate solution, and stirring for reaction; and finally, adding the mixed solution B, stirring and reacting until the solution is in a transparent state, thereby obtaining the hydrophobic and oleophobic liquid hardener. The product prepared by the preparation method disclosed by the invention has a relatively good anti-permeability effect.
本发明属于建筑施工材料技术领域，公开了一种疏水疏油型液体硬化剂及其制备方法；其中，所述制备方法包括：在40℃～70℃下，将活性硅粉水溶液加入到有机无机复合碱的水溶液，搅拌反应；过滤，得到无色透明液体A；在第一搅拌状态下，将醇类物质加入氟烷基丙烯酸酯共聚物，并控制pH值为7～9；在得到的溶液中边搅拌边加入硅烷偶联剂，得到混合溶液B；室温下，在第二搅拌状态下，将甲基硅酸钾加入所述无色透明液体A中，搅拌反应；然后，加入硅酸锂溶液，搅拌反应；最后，加入所述混合溶液B，搅拌反应直到溶液为透明状态，得到疏水疏油型液体硬化剂。本发明公开的制备方法制备获得的产品，具有较好的抗渗油效果。
Hydrophobic and oleophobic liquid hardening agent and preparation method thereof
一种疏水疏油型液体硬化剂及其制备方法
CAO HENG (author) / MENG PINGFAN (author)
2024-06-18
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
| European Patent Office | 2015
Hydrophobic and oleophobic film layer and preparation method thereof
| European Patent Office | 2024
Hydrophobic and Oleophobic Coatings
| Springer Verlag | 2004
Preparation and characterization of super-hydrophobic and oleophobic surface
| British Library Online Contents | 2010
Hydrophobic and oleophobic treatment method for silicon carbide ceramic membrane
| European Patent Office | 2021