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Zirconium magnesium phosphate solid electrolyte target material of thin-film magnesium battery, preparation method of zirconium magnesium phosphate solid electrolyte target material and battery
The invention relates to a magnesium zirconium phosphate solid electrolyte target of a thin-film magnesium battery, a preparation method and the thin-film magnesium battery, and belongs to the technical field of magnesium batteries. Comprising the following steps: mixing magnesium salt powder with phosphorus pentoxide and zirconium oxide powder to obtain mixed powder; putting the mixed powder into a closed ball milling tank, mixing with zirconium oxide balls, adding a dispersing agent, continuously mixing, and carrying out ball milling; then adding a binder into the ball milling tank, and continuing ball milling; sieving the ball-milled synthetic powder with a 500-mesh sieve, pouring the sieved synthetic powder into a vibration mold, and pressurizing to form a mold-pressed blank; putting the blank into a cold isostatic press, pressurizing and maintaining the pressure to obtain a magnesium zirconium phosphate solid electrolyte target blank subjected to cold isostatic pressing; and putting the magnesium zirconium phosphate solid electrolyte target blank into an atmosphere sintering furnace or a vacuum sintering furnace, carrying out multi-section heat preservation, and naturally cooling to room temperature along with the furnace to obtain the magnesium zirconium phosphate solid electrolyte target of the thin-film magnesium battery. The solid electrolyte target material disclosed by the invention is uniform in component and convenient for thin film deposition.
本发明涉及薄膜镁电池磷酸锆镁固态电解质靶材、制备方法及薄膜镁电池，属于镁电池技术领域。包括：将镁盐粉末与五氧化二磷和氧化锆粉末混合得到混合粉末；将混合粉末放入密闭球磨罐内与氧化锆球相混合，然后添加分散剂继续混合、球磨；然后在球磨罐添加粘结剂，继续球磨；球磨后的合成粉过500目的筛，过筛的合成粉倒入震动模具内，加压，形成模压的坯料；将坯料放入冷等静压机内加压并保压，得到冷等静压后的磷酸锆镁固态电解质靶材坯料；将磷酸锆镁固态电解质靶材坯料放入气氛烧结炉内或者放入真空烧结炉内，多段保温后，随炉自然冷却到室温，得到薄膜镁电池磷酸锆镁固态电解质靶材。本发明的固态电解质靶材的成分均匀，便于薄膜沉积。
Zirconium magnesium phosphate solid electrolyte target material of thin-film magnesium battery, preparation method of zirconium magnesium phosphate solid electrolyte target material and battery
The invention relates to a magnesium zirconium phosphate solid electrolyte target of a thin-film magnesium battery, a preparation method and the thin-film magnesium battery, and belongs to the technical field of magnesium batteries. Comprising the following steps: mixing magnesium salt powder with phosphorus pentoxide and zirconium oxide powder to obtain mixed powder; putting the mixed powder into a closed ball milling tank, mixing with zirconium oxide balls, adding a dispersing agent, continuously mixing, and carrying out ball milling; then adding a binder into the ball milling tank, and continuing ball milling; sieving the ball-milled synthetic powder with a 500-mesh sieve, pouring the sieved synthetic powder into a vibration mold, and pressurizing to form a mold-pressed blank; putting the blank into a cold isostatic press, pressurizing and maintaining the pressure to obtain a magnesium zirconium phosphate solid electrolyte target blank subjected to cold isostatic pressing; and putting the magnesium zirconium phosphate solid electrolyte target blank into an atmosphere sintering furnace or a vacuum sintering furnace, carrying out multi-section heat preservation, and naturally cooling to room temperature along with the furnace to obtain the magnesium zirconium phosphate solid electrolyte target of the thin-film magnesium battery. The solid electrolyte target material disclosed by the invention is uniform in component and convenient for thin film deposition.
本发明涉及薄膜镁电池磷酸锆镁固态电解质靶材、制备方法及薄膜镁电池，属于镁电池技术领域。包括：将镁盐粉末与五氧化二磷和氧化锆粉末混合得到混合粉末；将混合粉末放入密闭球磨罐内与氧化锆球相混合，然后添加分散剂继续混合、球磨；然后在球磨罐添加粘结剂，继续球磨；球磨后的合成粉过500目的筛，过筛的合成粉倒入震动模具内，加压，形成模压的坯料；将坯料放入冷等静压机内加压并保压，得到冷等静压后的磷酸锆镁固态电解质靶材坯料；将磷酸锆镁固态电解质靶材坯料放入气氛烧结炉内或者放入真空烧结炉内，多段保温后，随炉自然冷却到室温，得到薄膜镁电池磷酸锆镁固态电解质靶材。本发明的固态电解质靶材的成分均匀，便于薄膜沉积。
Zirconium magnesium phosphate solid electrolyte target material of thin-film magnesium battery, preparation method of zirconium magnesium phosphate solid electrolyte target material and battery
薄膜镁电池磷酸锆镁固态电解质靶材、制备方法及电池
ZHOU JUN (author) / LIU XIAOWEI (author) / MA GUILONG (author) / GAN ZHIJIAN (author) / LI WEIWEI (author)
2024-08-23
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
/
C23C
Beschichten metallischer Werkstoffe
,
COATING METALLIC MATERIAL
/
H01M
Verfahren oder Mittel, z.B. Batterien, für die direkte Umwandlung von chemischer in elektrische Energie
,
PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
Zirconium magnesium phosphate solid electrolyte target annealing method, target and battery
| European Patent Office | 2024
| European Patent Office | 2024
| European Patent Office | 2024
| European Patent Office | 2024
| European Patent Office | 2024