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Large-strain piezoelectric ceramic material and preparation method thereof
The invention discloses a preparation method of a large-strain piezoelectric ceramic material, which comprises the following steps: synthesizing glass powder with the component of (1-x) Pb (ZraTi1-a) O3-x (Bi0. 5Na0. 5) TiO3-ywt% BaZrO3-betawt% B2O3 by using a melting-water quenching method, x and a are molar ratios, and y and beta are mass ratios; the preparation method comprises the following steps: synthesizing ceramic powder of which the component is (1-x) Pb (ZraTi1-a) O3-x (Bi0. 5Na0. 5) TiO3-ywt% BaZrO3 by using a solid-phase synthesis method; the glass powder and the ceramic powder are used for preparing the (1-x) Pb (ZraTi1-a) O3-x (Bi < 0.5 > Na < 0.5 >) TiO < 3-y > BaZrO < 3-z > GL piezoelectric ceramic material by a solid-phase sintering method, and the composition of GL is (1-x) Pb (ZraTi1-a) O3-x (Bi < 0.5 > Na < 0.5 >) TiO < 3-y > wt% BaZrO < 3-beta > wt% B2O3. The special glass component is added into the PZT-based piezoelectric ceramic for modification, so that the strain of the material is remarkably improved while the microstructure of the ceramic material is optimized.
本发明公开了一种大应变压电陶瓷材料的制备方法，包括：利用熔融‑水淬法合成组分为(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑ywt％BaZrO3‑βwt％B2O3的玻璃粉体，其中，x、a为摩尔比，y、β为质量比；利用固相合成法合成组分为(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑ywt％BaZrO3的陶瓷粉体；利用所述玻璃粉体和所述陶瓷粉体，采用固相烧结法制备(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑yBaZrO3‑zGL压电陶瓷材料，其中，GL的组成为(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑ywt％BaZrO3‑βwt％B2O3。本发明通过向PZT基压电陶瓷中添加特制玻璃组分进行改性，在优化陶瓷材料微观结构的同时，显著提高了材料的应变。
Large-strain piezoelectric ceramic material and preparation method thereof
The invention discloses a preparation method of a large-strain piezoelectric ceramic material, which comprises the following steps: synthesizing glass powder with the component of (1-x) Pb (ZraTi1-a) O3-x (Bi0. 5Na0. 5) TiO3-ywt% BaZrO3-betawt% B2O3 by using a melting-water quenching method, x and a are molar ratios, and y and beta are mass ratios; the preparation method comprises the following steps: synthesizing ceramic powder of which the component is (1-x) Pb (ZraTi1-a) O3-x (Bi0. 5Na0. 5) TiO3-ywt% BaZrO3 by using a solid-phase synthesis method; the glass powder and the ceramic powder are used for preparing the (1-x) Pb (ZraTi1-a) O3-x (Bi < 0.5 > Na < 0.5 >) TiO < 3-y > BaZrO < 3-z > GL piezoelectric ceramic material by a solid-phase sintering method, and the composition of GL is (1-x) Pb (ZraTi1-a) O3-x (Bi < 0.5 > Na < 0.5 >) TiO < 3-y > wt% BaZrO < 3-beta > wt% B2O3. The special glass component is added into the PZT-based piezoelectric ceramic for modification, so that the strain of the material is remarkably improved while the microstructure of the ceramic material is optimized.
本发明公开了一种大应变压电陶瓷材料的制备方法，包括：利用熔融‑水淬法合成组分为(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑ywt％BaZrO3‑βwt％B2O3的玻璃粉体，其中，x、a为摩尔比，y、β为质量比；利用固相合成法合成组分为(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑ywt％BaZrO3的陶瓷粉体；利用所述玻璃粉体和所述陶瓷粉体，采用固相烧结法制备(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑yBaZrO3‑zGL压电陶瓷材料，其中，GL的组成为(1‑x)Pb(ZraTi1‑a)O3‑x(Bi0.5Na0.5)TiO3‑ywt％BaZrO3‑βwt％B2O3。本发明通过向PZT基压电陶瓷中添加特制玻璃组分进行改性，在优化陶瓷材料微观结构的同时，显著提高了材料的应变。
Large-strain piezoelectric ceramic material and preparation method thereof
一种大应变压电陶瓷材料及其制备方法
LI ZHIMIN (author) / JIANG DENGHUI (author) / PEI KAO (author)
2024-10-29
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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