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MANUFACTURING METHOD OF SINTERED BODY, AND SINTERED BODY
To provide a manufacturing method of a porous sintered body having conductivity degradation suppressed, and a sintered body.SOLUTION: A manufacturing method of a sintered body includes a precursor manufacturing step for burning powder obtained by mixing lithium hydroxide and basic material powder of a garnet type oxide containing at least Li, La, and Zr and having an average particle size in the range of 0.1 μm or more and 5 μm or less to synthesize precursor powder not sintered yet and a molding and sintering step for molding the precursor powder as it is or after added with a pore-forming agent and sintering the obtained molded article at a temperature of 900°C or lower to manufacture a sintered body having a void of 8 vol.% or more.SELECTED DRAWING: None
【課題】多孔性を有し、伝導度の低下をより抑制する焼結体の製造方法及び焼結体を提供する。【解決手段】焼結体の製造方法は、平均粒径が0.1μm以上5μm以下の範囲でありLiとLaとZrと少なくとも含むガーネット型酸化物の母材粉末と、水酸化リチウムとを混合して得られた粉末を焼成して未焼結の前駆体粉末を合成する前駆体製造工程と、前駆体粉末をそのまま成形するか又は前駆体粉末に造孔材を添加して成形し得られた成形体を900℃以下の温度で焼結させ空隙を8体積%以上有する焼結体を得る成形焼結工程と、を含む。【選択図】なし
MANUFACTURING METHOD OF SINTERED BODY, AND SINTERED BODY
To provide a manufacturing method of a porous sintered body having conductivity degradation suppressed, and a sintered body.SOLUTION: A manufacturing method of a sintered body includes a precursor manufacturing step for burning powder obtained by mixing lithium hydroxide and basic material powder of a garnet type oxide containing at least Li, La, and Zr and having an average particle size in the range of 0.1 μm or more and 5 μm or less to synthesize precursor powder not sintered yet and a molding and sintering step for molding the precursor powder as it is or after added with a pore-forming agent and sintering the obtained molded article at a temperature of 900°C or lower to manufacture a sintered body having a void of 8 vol.% or more.SELECTED DRAWING: None
【課題】多孔性を有し、伝導度の低下をより抑制する焼結体の製造方法及び焼結体を提供する。【解決手段】焼結体の製造方法は、平均粒径が0.1μm以上5μm以下の範囲でありLiとLaとZrと少なくとも含むガーネット型酸化物の母材粉末と、水酸化リチウムとを混合して得られた粉末を焼成して未焼結の前駆体粉末を合成する前駆体製造工程と、前駆体粉末をそのまま成形するか又は前駆体粉末に造孔材を添加して成形し得られた成形体を900℃以下の温度で焼結させ空隙を8体積%以上有する焼結体を得る成形焼結工程と、を含む。【選択図】なし
MANUFACTURING METHOD OF SINTERED BODY, AND SINTERED BODY
焼結体の製造方法及び焼結体
YAMAKAWA SHUNSUKE (author) / OTA SHINGO (author) / WATANABE MASAKI (author) / HAYASHI MASAHIRO (author) / TAKAHASHI KEITA (author)
2021-02-18
Patent
Electronic Resource
Japanese
IPC:
C04B
Kalk
,
LIME
/
C01G
Verbindungen der von den Unterklassen C01D oder C01F nicht umfassten Metalle
,
COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
/
H01B
CABLES
,
Kabel
/
H01M
Verfahren oder Mittel, z.B. Batterien, für die direkte Umwandlung von chemischer in elektrische Energie
,
PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
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