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Microporous and Hierarchical ZSM-5 Zeolites in Friedländer Synthesis

Grigor’eva, N. G. / Bubennov, S. V. / Artem’eva, A. S. / Serebrennikov, D. V. / Filippova, N. A. / Kutepov, B. I.

The study investigates the catalytic performance of microporous and granular micro–meso–macroporous zeolites (H-ZSM-5 and H-ZSM-5h, respectively) in synthesis of quinolines by the reaction of 2-aminoacetophenone with diketones (2,4-pentanedione or dimedone), known as the Friedländer synthesis. In the presence of H-ZSM-5h, 1-(2,4-dimethylquinolin-3-yl)ethanone (1a) and 3,4-dihydro-3,3,9-trimethyl-1(2H)-acridinone (1b) were produced in 82 and 93% yields, respectively.

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Microporous and Hierarchical ZSM-5 Zeolites in Friedländer Synthesis

Grigor’eva, N. G. / Bubennov, S. V. / Artem’eva, A. S. / Serebrennikov, D. V. / Filippova, N. A. / Kutepov, B. I.

The study investigates the catalytic performance of microporous and granular micro–meso–macroporous zeolites (H-ZSM-5 and H-ZSM-5h, respectively) in synthesis of quinolines by the reaction of 2-aminoacetophenone with diketones (2,4-pentanedione or dimedone), known as the Friedländer synthesis. In the presence of H-ZSM-5h, 1-(2,4-dimethylquinolin-3-yl)ethanone (1a) and 3,4-dihydro-3,3,9-trimethyl-1(2H)-acridinone (1b) were produced in 82 and 93% yields, respectively.

Microporous and Hierarchical ZSM-5 Zeolites in Friedländer Synthesis

Grigor’eva, N. G. / Bubennov, S. V. / Artem’eva, A. S. / Serebrennikov, D. V. / Filippova, N. A. / Kutepov, B. I.

The study investigates the catalytic performance of microporous and granular micro–meso–macroporous zeolites (H-ZSM-5 and H-ZSM-5h, respectively) in synthesis of quinolines by the reaction of 2-aminoacetophenone with diketones (2,4-pentanedione or dimedone), known as the Friedländer synthesis. In the presence of H-ZSM-5h, 1-(2,4-dimethylquinolin-3-yl)ethanone (1a) and 3,4-dihydro-3,3,9-trimethyl-1(2H)-acridinone (1b) were produced in 82 and 93% yields, respectively.

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Title:

Microporous and Hierarchical ZSM-5 Zeolites in Friedländer Synthesis

Additional title:

Pet. Chem.

Contributors:

Grigor’eva, N. G. (author) / Bubennov, S. V. (author) / Artem’eva, A. S. (author) / Serebrennikov, D. V. (author) / Filippova, N. A. (author) / Kutepov, B. I. (author)

Published in:

Petroleum Chemistry ; 63 ; 759-768

Publication date:

2023-07-01

Size:

10 pages

ISSN:

1555-6239 , 0965-5441

DOI:

https://doi.org/10.1134/S0965544123050092

Type of media:

Article (Journal)

Type of material:

Electronic Resource

Language:

English

Keywords:

Friedländer synthesis , zeolites , granular hierarchical zeolites , quinolines , acridinones Chemistry , Industrial Chemistry/Chemical Engineering , Chemistry and Materials Science

Licence:

http://creativecommons.org/licenses/by/4.0/

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