Eine Plattform für die Wissenschaft: Bauingenieurwesen, Architektur und Urbanistik
Eine Plattform für die Wissenschaft: Bauingenieurwesen, Architektur und Urbanistik
The invention discloses an alpha crystal form nano alumina porous ceramic with a high apparent porosity and a preparation method thereof, and belongs to the field of nano porous materials. The preparation method comprises the following steps: filling gamma-Al2O3 powder into a graphite mould, placing the mould into a discharging plasma sintering furnace, loading an axial load pressure of 30 to 100 MPa, sintering the powder in vacuum at a temperature of 1100 to 1250 DEG C, maintaining the temperature for 3 to 5 minutes; or placing a gamma-Al2O3 blank in a conventional air furnace, sintering the blank under zero pressure at a temperature of 1350 to 1450 DEG C, and maintaining the temperature for 30 to 120 minutes to obtain the alpha crystal form nano alumina porous ceramic with a high apparent porosity; wherein the average particle size of the porous ceramic is smaller than 160 nm, and the apparent porosity is more than 95%. The provided preparation method has the advantages of low cost and good repeatability. The porous structure is formed without any sintering aid or pore forming agent. The prepared alumina porous ceramic has the advantages of evenly-distributed pores, small pore diameter, high apparent porosity (more than 95%), and excellent mechanical properties.
The invention discloses an alpha crystal form nano alumina porous ceramic with a high apparent porosity and a preparation method thereof, and belongs to the field of nano porous materials. The preparation method comprises the following steps: filling gamma-Al2O3 powder into a graphite mould, placing the mould into a discharging plasma sintering furnace, loading an axial load pressure of 30 to 100 MPa, sintering the powder in vacuum at a temperature of 1100 to 1250 DEG C, maintaining the temperature for 3 to 5 minutes; or placing a gamma-Al2O3 blank in a conventional air furnace, sintering the blank under zero pressure at a temperature of 1350 to 1450 DEG C, and maintaining the temperature for 30 to 120 minutes to obtain the alpha crystal form nano alumina porous ceramic with a high apparent porosity; wherein the average particle size of the porous ceramic is smaller than 160 nm, and the apparent porosity is more than 95%. The provided preparation method has the advantages of low cost and good repeatability. The porous structure is formed without any sintering aid or pore forming agent. The prepared alumina porous ceramic has the advantages of evenly-distributed pores, small pore diameter, high apparent porosity (more than 95%), and excellent mechanical properties.
Alpha crystal form nano alumina porous ceramic with high apparent porosity and preparation method thereof
18.11.2015
Patent
Elektronische Ressource
Englisch
IPC:
C04B
Kalk
,
LIME
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