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Preparation device of scandium oxide stabilized zirconia powder
The invention provides a preparation device of scandium oxide stabilized zirconia powder. The device comprises a scandium-containing zirconium-containing solution supply unit, a precipitator supply unit, a microwave or ultrasonic reactor, a filtering unit, a washing unit, a drying unit and a calcining unit, wherein the microwave or ultrasonic reactor is used for carrying out coprecipitation reaction on the scandium-zirconium mixed solution under the condition of microwave heating or ultrasonic waves; the filtering unit is provided with a precipitated material inlet and a precipitated colloid outlet; the precipitated material inlet is connected with the microwave or ultrasonic reactor; the washing unit is provided with a precipitation colloid inlet, a washing liquid inlet and a washing colloid outlet; the precipitation colloid inlet is connected with the precipitation colloid outlet; the drying unit is provided with a washing colloid inlet and a dry material outlet; the washing colloidinlet is connected with the washing colloid outlet; and the calcining unit is used for calcining the dry material discharged by the drying unit to obtain scandium oxide stabilized zirconia powder. Byutilizing the device, the problem that scandium-zirconium powder prepared by a coprecipitation method is easy to agglomerate is effectively solved.
本发明提供了一种氧化钪稳定氧化锆粉体的制备装置。该装置包括含钪含锆溶液供应单元、沉淀剂供应单元、微波或超声波反应器、过滤单元、洗涤单元、干燥单元和煅烧单元;微波或超声波反应器用于使钪锆混合溶液在微波加热或超声波的条件下进行共沉淀反应;过滤单元具有沉淀物料进口和沉淀胶体出口,沉淀物料进口与微波或超声波反应器相连;洗涤单元具有沉淀胶体进口、洗涤液进口及洗涤胶体出口,沉淀胶体进口与沉淀胶体出口相连;干燥单元具有洗涤胶体进口和干料出口,洗涤胶体进口与洗涤胶体出口相连;煅烧单元用于对干燥单元排出的干料进行煅烧以得到氧化钪稳定氧化锆粉体。利用该装置有效解决了共沉淀法制备钪锆粉体存在的易团聚的问题。
Preparation device of scandium oxide stabilized zirconia powder
The invention provides a preparation device of scandium oxide stabilized zirconia powder. The device comprises a scandium-containing zirconium-containing solution supply unit, a precipitator supply unit, a microwave or ultrasonic reactor, a filtering unit, a washing unit, a drying unit and a calcining unit, wherein the microwave or ultrasonic reactor is used for carrying out coprecipitation reaction on the scandium-zirconium mixed solution under the condition of microwave heating or ultrasonic waves; the filtering unit is provided with a precipitated material inlet and a precipitated colloid outlet; the precipitated material inlet is connected with the microwave or ultrasonic reactor; the washing unit is provided with a precipitation colloid inlet, a washing liquid inlet and a washing colloid outlet; the precipitation colloid inlet is connected with the precipitation colloid outlet; the drying unit is provided with a washing colloid inlet and a dry material outlet; the washing colloidinlet is connected with the washing colloid outlet; and the calcining unit is used for calcining the dry material discharged by the drying unit to obtain scandium oxide stabilized zirconia powder. Byutilizing the device, the problem that scandium-zirconium powder prepared by a coprecipitation method is easy to agglomerate is effectively solved.
本发明提供了一种氧化钪稳定氧化锆粉体的制备装置。该装置包括含钪含锆溶液供应单元、沉淀剂供应单元、微波或超声波反应器、过滤单元、洗涤单元、干燥单元和煅烧单元;微波或超声波反应器用于使钪锆混合溶液在微波加热或超声波的条件下进行共沉淀反应;过滤单元具有沉淀物料进口和沉淀胶体出口,沉淀物料进口与微波或超声波反应器相连;洗涤单元具有沉淀胶体进口、洗涤液进口及洗涤胶体出口,沉淀胶体进口与沉淀胶体出口相连;干燥单元具有洗涤胶体进口和干料出口,洗涤胶体进口与洗涤胶体出口相连;煅烧单元用于对干燥单元排出的干料进行煅烧以得到氧化钪稳定氧化锆粉体。利用该装置有效解决了共沉淀法制备钪锆粉体存在的易团聚的问题。
Preparation device of scandium oxide stabilized zirconia powder
氧化钪稳定氧化锆粉体的制备装置
LI XIAOYAN (Autor:in) / FU YUNFENG (Autor:in) / WANG WEIWEI (Autor:in) / LI NUO (Autor:in) / LIU ZHAOBO (Autor:in) / FU GUOYAN (Autor:in)
12.05.2020
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
Scandium oxide stabilized zirconia powder and preparation method thereof
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