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Preparation method of thorium dioxide nano material
The invention discloses a preparation method of a thorium dioxide nano material, and belongs to the technical field of nano materials. The preparation method comprises the following steps: uniformly mixing a thorium nitrate solution and a sodium hydroxide solution, adding the mixture into a reaction kettle for hydrothermal reaction, cooling the reaction product to room temperature, washing the reaction product with water until the pH value is 7.5-8.5, and drying and grinding the reaction product to obtain the thorium dioxide nano material. By utilizing the preparation method of the thorium dioxide nano material, ThO2 ceramic nano powder with controllable morphology, light agglomeration, uniform particle size, high specific surface area and good catalytic activity can be prepared on a largescale.
本发明公开了一种二氧化钍纳米材料的制备方法,属于纳米材料技术领域。所述的制备方法是将硝酸钍溶液与氢氧化钠溶液混合均匀,加入反应釜中水热反应,反应产物冷却到室温后水洗涤至pH为7.5‑8.5,烘干研磨,即制得二氧化钍纳米材料。利用本发明的二氧化钍纳米材料的制备方法,能够大规模制备形貌可控、团聚较轻、粒径均匀、比表面积较高、催化活性好的ThO陶瓷纳米粉体。
Preparation method of thorium dioxide nano material
The invention discloses a preparation method of a thorium dioxide nano material, and belongs to the technical field of nano materials. The preparation method comprises the following steps: uniformly mixing a thorium nitrate solution and a sodium hydroxide solution, adding the mixture into a reaction kettle for hydrothermal reaction, cooling the reaction product to room temperature, washing the reaction product with water until the pH value is 7.5-8.5, and drying and grinding the reaction product to obtain the thorium dioxide nano material. By utilizing the preparation method of the thorium dioxide nano material, ThO2 ceramic nano powder with controllable morphology, light agglomeration, uniform particle size, high specific surface area and good catalytic activity can be prepared on a largescale.
本发明公开了一种二氧化钍纳米材料的制备方法,属于纳米材料技术领域。所述的制备方法是将硝酸钍溶液与氢氧化钠溶液混合均匀,加入反应釜中水热反应,反应产物冷却到室温后水洗涤至pH为7.5‑8.5,烘干研磨,即制得二氧化钍纳米材料。利用本发明的二氧化钍纳米材料的制备方法,能够大规模制备形貌可控、团聚较轻、粒径均匀、比表面积较高、催化活性好的ThO陶瓷纳米粉体。
Preparation method of thorium dioxide nano material
一种二氧化钍纳米材料的制备方法
ZHAO YAOLIN (Autor:in) / WANG BIAO (Autor:in) / ZUO FENG (Autor:in) / NIE SHAOWEI (Autor:in) / XIAO SONGTAO (Autor:in) / LIU XIECHUN (Autor:in) / JIANG LILI (Autor:in)
04.09.2020
Patent
Elektronische Ressource
Chinesisch
IPC:
C01F
COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
,
Verbindungen der Metalle Beryllium, Magnesium, Aluminium, Calcium, Strontium, Barium, Radium, Thorium oder der Seltenen Erden
/
B01J
Chemische oder physikalische Verfahren, z.B. Katalyse oder Kolloidchemie
,
CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY
/
B82Y
Bestimmter Gebrauch oder bestimmte Anwendung von Nanostrukturen
,
SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES
/
C04B
Kalk
,
LIME
/
G21C
NUCLEAR REACTORS
,
Kernreaktoren
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