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Preparation method of ZrSiO4 anti-oxidation coating on surface of SiC fiber
The invention discloses a preparation method of a ZrSiO4 anti-oxidation coating on a SiC fiber surface. The preparation method comprises the following steps: (1) preparing a ZrSiO4 precursor steeping liquor, reacting and aging; (2) removing glue on the surface of the SiC fiber; (3) carrying out dip-coating on the SiC fiber by using the ZrSiO4 precursor steeping liquor; (4) drying the ZrSiO4 precursor; (5) high-temperature cracking of the ZrSiO4 precursor, the ZrSiO4 coating on the surface of the SiC fiber is prepared through the method, the high-temperature oxidation weight gain rate of the SiC fiber is obviously reduced, and it is indicated that the prepared ZrSiO4 coating can play a remarkable anti-oxidation protection role on the SiC fiber.
本发明公开了一种SiC纤维表面ZrSiO4抗氧化涂层的制备方法,包括(1)ZrSiO4前驱体浸渍液的配制、反应与陈化;(2)SiC纤维表面除胶处理;(3)使用ZrSiO4前驱体浸渍液浸涂SiC纤维;(4)ZrSiO4前驱体干燥;(5)ZrSiO4前驱体高温裂解,本发明通过该方法制备SiC纤维表面的ZrSiO4涂层,明显降低SiC纤维的高温氧化增重率,说明所制备的ZrSiO4涂层可对SiC纤维起到显著的抗氧化保护作用。
Preparation method of ZrSiO4 anti-oxidation coating on surface of SiC fiber
The invention discloses a preparation method of a ZrSiO4 anti-oxidation coating on a SiC fiber surface. The preparation method comprises the following steps: (1) preparing a ZrSiO4 precursor steeping liquor, reacting and aging; (2) removing glue on the surface of the SiC fiber; (3) carrying out dip-coating on the SiC fiber by using the ZrSiO4 precursor steeping liquor; (4) drying the ZrSiO4 precursor; (5) high-temperature cracking of the ZrSiO4 precursor, the ZrSiO4 coating on the surface of the SiC fiber is prepared through the method, the high-temperature oxidation weight gain rate of the SiC fiber is obviously reduced, and it is indicated that the prepared ZrSiO4 coating can play a remarkable anti-oxidation protection role on the SiC fiber.
本发明公开了一种SiC纤维表面ZrSiO4抗氧化涂层的制备方法,包括(1)ZrSiO4前驱体浸渍液的配制、反应与陈化;(2)SiC纤维表面除胶处理;(3)使用ZrSiO4前驱体浸渍液浸涂SiC纤维;(4)ZrSiO4前驱体干燥;(5)ZrSiO4前驱体高温裂解,本发明通过该方法制备SiC纤维表面的ZrSiO4涂层,明显降低SiC纤维的高温氧化增重率,说明所制备的ZrSiO4涂层可对SiC纤维起到显著的抗氧化保护作用。
Preparation method of ZrSiO4 anti-oxidation coating on surface of SiC fiber
一种SiC纤维表面ZrSiO4抗氧化涂层的制备方法
YANG HUIYONG (Autor:in) / LIU RONGJUN (Autor:in) / ZHOU XINGUI (Autor:in) / WANG HONGLEI (Autor:in) / CHEN DIAN (Autor:in) / XU BIN (Autor:in) / LUO RUIYING (Autor:in) / WANG LIANYI (Autor:in) / HUANG JUNTONG (Autor:in) / CHEN ZHI (Autor:in)
06.05.2022
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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