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Bismuth borosilicate glass coated fine grain barium titanate ceramic dielectric material and preparation method thereof
The invention relates to a bismuth borosilicate glass coated fine grain barium titanate ceramic dielectric material and a preparation method thereof. The preparation method comprises the following steps: preparing bismuth borosilicate glass sol by using a sol-gel method, wherein bismuth borosilicate glass is Bi2O3-B2O3-SiO2 glass; the preparation method comprises the following steps: dispersing BaTiO3 powder into bismuth borosilicate glass sol to obtain BaTiO3 powder coated with the bismuth borosilicate glass sol; and calcining the bismuth borosilicate glass sol coated BaTiO3 powder to obtain the bismuth borosilicate glass coated fine grain barium titanate ceramic powder. Granulating and forming the bismuth borosilicate glass coated fine-grain barium titanate ceramic powder to obtain a barium titanate ceramic green body, and heating to obtain fine-grain barium titanate dielectric ceramic, namely the bismuth borosilicate glass coated fine-grain barium titanate ceramic dielectric material. Compared with the prior art, the glass-coated BaTiO3 powder is prepared by a sol-gel method to form the core-shell structure powder, and the core-shell structure powder of the glass-coated BaTiO3 powder is used for preparing fine grain barium titanate ceramic and can be widely applied to the field of application of electronic materials.
本发明涉及铋硼硅玻璃包覆的细晶钛酸钡陶瓷介质材料及其制备方法。用溶胶凝胶法制备铋硼硅玻璃溶胶,所述铋硼硅玻璃为Bi2O3‑B2O3‑SiO2玻璃;将BaTiO3粉体分散于铋硼硅玻璃溶胶中,得到铋硼硅玻璃溶胶包覆的BaTiO3粉体;铋硼硅玻璃溶胶包覆的BaTiO3粉体经煅烧后,得到铋硼硅玻璃包覆的细晶钛酸钡陶瓷粉。铋硼硅玻璃包覆的细晶钛酸钡陶瓷粉经造粒、成型,得到钛酸钡陶瓷生坯,升温得到细晶的钛酸钡介质陶瓷,即为铋硼硅玻璃包覆的细晶钛酸钡陶瓷介质材料。与现有技术相比,本发明通过溶胶凝胶法制备玻璃包覆BaTiO3粉形成核壳结构粉体,该种玻璃包覆BaTiO3粉的核壳结构粉体用于细晶钛酸钡陶瓷的制备,可以广泛适用于电子材料应用领域。
Bismuth borosilicate glass coated fine grain barium titanate ceramic dielectric material and preparation method thereof
The invention relates to a bismuth borosilicate glass coated fine grain barium titanate ceramic dielectric material and a preparation method thereof. The preparation method comprises the following steps: preparing bismuth borosilicate glass sol by using a sol-gel method, wherein bismuth borosilicate glass is Bi2O3-B2O3-SiO2 glass; the preparation method comprises the following steps: dispersing BaTiO3 powder into bismuth borosilicate glass sol to obtain BaTiO3 powder coated with the bismuth borosilicate glass sol; and calcining the bismuth borosilicate glass sol coated BaTiO3 powder to obtain the bismuth borosilicate glass coated fine grain barium titanate ceramic powder. Granulating and forming the bismuth borosilicate glass coated fine-grain barium titanate ceramic powder to obtain a barium titanate ceramic green body, and heating to obtain fine-grain barium titanate dielectric ceramic, namely the bismuth borosilicate glass coated fine-grain barium titanate ceramic dielectric material. Compared with the prior art, the glass-coated BaTiO3 powder is prepared by a sol-gel method to form the core-shell structure powder, and the core-shell structure powder of the glass-coated BaTiO3 powder is used for preparing fine grain barium titanate ceramic and can be widely applied to the field of application of electronic materials.
本发明涉及铋硼硅玻璃包覆的细晶钛酸钡陶瓷介质材料及其制备方法。用溶胶凝胶法制备铋硼硅玻璃溶胶,所述铋硼硅玻璃为Bi2O3‑B2O3‑SiO2玻璃;将BaTiO3粉体分散于铋硼硅玻璃溶胶中,得到铋硼硅玻璃溶胶包覆的BaTiO3粉体;铋硼硅玻璃溶胶包覆的BaTiO3粉体经煅烧后,得到铋硼硅玻璃包覆的细晶钛酸钡陶瓷粉。铋硼硅玻璃包覆的细晶钛酸钡陶瓷粉经造粒、成型,得到钛酸钡陶瓷生坯,升温得到细晶的钛酸钡介质陶瓷,即为铋硼硅玻璃包覆的细晶钛酸钡陶瓷介质材料。与现有技术相比,本发明通过溶胶凝胶法制备玻璃包覆BaTiO3粉形成核壳结构粉体,该种玻璃包覆BaTiO3粉的核壳结构粉体用于细晶钛酸钡陶瓷的制备,可以广泛适用于电子材料应用领域。
Bismuth borosilicate glass coated fine grain barium titanate ceramic dielectric material and preparation method thereof
铋硼硅玻璃包覆的细晶钛酸钡陶瓷介质材料及其制备方法
ZENG HUIDAN (Autor:in) / YU JIA (Autor:in) / ZHANG SHENRUI (Autor:in)
13.02.2024
Patent
Elektronische Ressource
Chinesisch
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