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Lead calcium zirconate stannate ceramic as well as preparation method and application thereof
The invention provides a lead calcium zirconate stannate ceramic and a preparation method and application thereof, and relates to the technical field of dielectric energy storage materials, the lead calcium zirconate stannate ceramic is synthesized and prepared through a traditional solid-phase reaction method and a two-stage sintering process, the chemical component of the ceramic is (Pb < 1-x > Cax) (Zr < 0.55 > Sn < 0.45 >) O < 3 > (PCZS), and x is 0.01, 0.02, 0.03 or 0.04. The PCZS ceramic powder with different Ca < 2 + > doping amounts synthesized by the invention is of a pure perovskite structure, the distribution and the size of sintered crystal grains of a sample are uniform and compact, the dielectric loss in a low-temperature section is lower than 3%, and the ceramic component has good frequency stability in a frequency band of 50kHz-1000kHz; the high energy storage density and energy storage efficiency of the material are of great significance in realizing large-scale integrated circuits.
本发明提供一种锆锡酸钙铅陶瓷及其制备方法和应用,涉及电介质储能材料技术领域,本发明通过传统固相反应法和二段烧结工艺合成并制备锆锡酸钙铅陶瓷,陶瓷化学成分为(Pb1‑xCax)(Zr0.55Sn0.45)O3(PCZS),x取0.01、0.02、0.03、0.04。本发明合成的不同Ca2+掺量的PCZS陶瓷粉体,为纯钙钛矿结构,样品烧结晶粒分布和尺寸均匀致密,在低温段介电损耗低于3%,并且在50kHz~1000kHz频率段该陶瓷组分具有良好的频率稳定性,其表现出的高的储能密度和储能效率在实现大规模集成电路具有重大意义。
Lead calcium zirconate stannate ceramic as well as preparation method and application thereof
The invention provides a lead calcium zirconate stannate ceramic and a preparation method and application thereof, and relates to the technical field of dielectric energy storage materials, the lead calcium zirconate stannate ceramic is synthesized and prepared through a traditional solid-phase reaction method and a two-stage sintering process, the chemical component of the ceramic is (Pb < 1-x > Cax) (Zr < 0.55 > Sn < 0.45 >) O < 3 > (PCZS), and x is 0.01, 0.02, 0.03 or 0.04. The PCZS ceramic powder with different Ca < 2 + > doping amounts synthesized by the invention is of a pure perovskite structure, the distribution and the size of sintered crystal grains of a sample are uniform and compact, the dielectric loss in a low-temperature section is lower than 3%, and the ceramic component has good frequency stability in a frequency band of 50kHz-1000kHz; the high energy storage density and energy storage efficiency of the material are of great significance in realizing large-scale integrated circuits.
本发明提供一种锆锡酸钙铅陶瓷及其制备方法和应用,涉及电介质储能材料技术领域,本发明通过传统固相反应法和二段烧结工艺合成并制备锆锡酸钙铅陶瓷,陶瓷化学成分为(Pb1‑xCax)(Zr0.55Sn0.45)O3(PCZS),x取0.01、0.02、0.03、0.04。本发明合成的不同Ca2+掺量的PCZS陶瓷粉体,为纯钙钛矿结构,样品烧结晶粒分布和尺寸均匀致密,在低温段介电损耗低于3%,并且在50kHz~1000kHz频率段该陶瓷组分具有良好的频率稳定性,其表现出的高的储能密度和储能效率在实现大规模集成电路具有重大意义。
Lead calcium zirconate stannate ceramic as well as preparation method and application thereof
一种锆锡酸钙铅陶瓷及其制备方法和应用
LU SHENGGUO (Autor:in) / YU CHAO (Autor:in) / WANG SHIBIN (Autor:in) / LI WEIQIU (Autor:in) / YU YULIANG (Autor:in)
27.02.2024
Patent
Elektronische Ressource
Chinesisch
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