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3D printing normal-pressure solid-phase sintered silicon carbide ceramic and preparation method thereof
The invention relates to a 3D printing normal-pressure solid-phase sintered silicon carbide ceramic and a preparation method thereof. The preparation method of the 3D printing normal-pressure solid-phase sintered silicon carbide ceramic comprises the following steps: (1) mixing silicon carbide ceramic powder, a boron-containing sintering aid, a carbon-containing sintering aid and a surfactant in a solvent to obtain mixed slurry, and drying, crushing and sieving the mixed slurry to obtain ceramic modified raw material powder; (2) preheating the ceramic modified raw material powder in an internal mixer, then adding a binder and mixing to obtain pug, and cooling and granulating to obtain a granular printing material; (3) molding the granular printing material through an FDM 3D printing process to obtain a silicon carbide ceramic biscuit; and (4) degreasing the silicon carbide ceramic biscuit to remove the binder, and performing normal-pressure solid-phase sintering densification to obtain the 3D printing normal-pressure solid-phase sintered silicon carbide ceramic.
本发明涉及一种3D打印常压固相烧结碳化硅陶瓷及其制备方法。所述3D打印常压固相烧结碳化硅陶瓷的制备方法包括以下步骤:(1)将碳化硅陶瓷粉体、含硼烧结助剂、含碳烧结助剂、表面活性剂在溶剂中混合得到混合浆料,经干燥、破碎、过筛,得到陶瓷改性原料粉体;(2)将陶瓷改性原料粉体在密炼机中预热,然后加入粘结剂并进行混炼,得到泥料,经冷却、造粒,得到颗粒状打印料;(3)将颗粒状打印料通过FDM 3D打印工艺成型,得到碳化硅陶瓷素坯;(4)将碳化硅陶瓷素坯进行脱脂除去粘结剂,常压固相烧结致密化,得到所述3D打印常压固相烧结碳化硅陶瓷。
3D printing normal-pressure solid-phase sintered silicon carbide ceramic and preparation method thereof
The invention relates to a 3D printing normal-pressure solid-phase sintered silicon carbide ceramic and a preparation method thereof. The preparation method of the 3D printing normal-pressure solid-phase sintered silicon carbide ceramic comprises the following steps: (1) mixing silicon carbide ceramic powder, a boron-containing sintering aid, a carbon-containing sintering aid and a surfactant in a solvent to obtain mixed slurry, and drying, crushing and sieving the mixed slurry to obtain ceramic modified raw material powder; (2) preheating the ceramic modified raw material powder in an internal mixer, then adding a binder and mixing to obtain pug, and cooling and granulating to obtain a granular printing material; (3) molding the granular printing material through an FDM 3D printing process to obtain a silicon carbide ceramic biscuit; and (4) degreasing the silicon carbide ceramic biscuit to remove the binder, and performing normal-pressure solid-phase sintering densification to obtain the 3D printing normal-pressure solid-phase sintered silicon carbide ceramic.
本发明涉及一种3D打印常压固相烧结碳化硅陶瓷及其制备方法。所述3D打印常压固相烧结碳化硅陶瓷的制备方法包括以下步骤:(1)将碳化硅陶瓷粉体、含硼烧结助剂、含碳烧结助剂、表面活性剂在溶剂中混合得到混合浆料,经干燥、破碎、过筛,得到陶瓷改性原料粉体;(2)将陶瓷改性原料粉体在密炼机中预热,然后加入粘结剂并进行混炼,得到泥料,经冷却、造粒,得到颗粒状打印料;(3)将颗粒状打印料通过FDM 3D打印工艺成型,得到碳化硅陶瓷素坯;(4)将碳化硅陶瓷素坯进行脱脂除去粘结剂,常压固相烧结致密化,得到所述3D打印常压固相烧结碳化硅陶瓷。
3D printing normal-pressure solid-phase sintered silicon carbide ceramic and preparation method thereof
一种3D打印常压固相烧结碳化硅陶瓷及其制备方法
HUANG ZHENGREN (Autor:in) / CHEN JIAN (Autor:in) / GAO CHENXI (Autor:in) / HUANG CHANGCONG (Autor:in) / LIAO SHENGJUN (Autor:in) / PENG LAN (Autor:in) / CHEN ZHONGMING (Autor:in)
11.10.2024
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
/
B33Y
ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
,
Additive (generative) Fertigung, d. h. die Herstellung von dreidimensionalen [3D] Bauteilen durch additive Abscheidung, additive Agglomeration oder additive Schichtung, z. B. durch 3D- Drucken, Stereolithografie oder selektives Lasersintern
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