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Resource utilization method of 1-aminoanthraquinone and DSD acid production wastewater
The invention discloses a resource utilization method of 1-aminoanthraquinone and DSD acid production wastewater. The method comprises the steps of: 1, adding production wastewater, a sulfonating agent, phenol, water and sodium hydroxide into a reaction kettle, performing dissolving and stirring, and mixing the substances uniformly; 2, dropwise adding acetone, carrying out sulfonation reaction, and starting to add a formaldehyde solution dropwise after the sulfonation reaction is finished; 3, conducting heat preservation at the end of dropwise adding; and 4, acquiring a concrete water reducingagent or a coal water slurry dispersing agent at the end of the heat preservation. Specifically, the wastewater in the step 1 is one or two of 1-aminoanthraquinone production wastewater and DSD acidproduction wastewater; a sulfonated acetone formaldehyde condensate or an aminosulfonic acid series formaldehyde condensate is subjected to graft modification, so that the water reducing effect and the dispersing effect are enhanced; pollution and damage to the environment and the human body are prevented, meanwhile, direct cyclic utilization can be achieved, energy consumption is reduced, and secondary pollution and resource waste cannot be caused; the production cost of the water reducing agent or the dispersing agent is reduced.
本发明公开了一种1‑氨基蒽醌和DSD酸生产废水的资源化利用方法，所述方法包括如下步骤：步骤一，向反应釜中加入所述生产废水、磺化剂、苯酚、水、氢氧化钠，溶解搅拌混合均匀；步骤二，滴加丙酮，进行磺化反应，磺化反应结束后开始滴加甲醛溶液；步骤三，滴加完毕后进行保温；步骤四，保温结束即得混凝土减水剂或者水煤浆分散剂；所述步骤一中废水为1‑氨基蒽醌生产废水和DSD酸生产废水中的一种或者两种；对磺化丙酮甲醛缩合物或者氨基磺酸系甲醛缩合物进行接枝改性，增强了减水效果和分散效果；防止其对环境、对人体造成污染与损害，同时可直接循环利用，节省能耗，不会造成二次污染和资源的浪费；降低了减水剂或者分散剂的生产成本。
Resource utilization method of 1-aminoanthraquinone and DSD acid production wastewater
The invention discloses a resource utilization method of 1-aminoanthraquinone and DSD acid production wastewater. The method comprises the steps of: 1, adding production wastewater, a sulfonating agent, phenol, water and sodium hydroxide into a reaction kettle, performing dissolving and stirring, and mixing the substances uniformly; 2, dropwise adding acetone, carrying out sulfonation reaction, and starting to add a formaldehyde solution dropwise after the sulfonation reaction is finished; 3, conducting heat preservation at the end of dropwise adding; and 4, acquiring a concrete water reducingagent or a coal water slurry dispersing agent at the end of the heat preservation. Specifically, the wastewater in the step 1 is one or two of 1-aminoanthraquinone production wastewater and DSD acidproduction wastewater; a sulfonated acetone formaldehyde condensate or an aminosulfonic acid series formaldehyde condensate is subjected to graft modification, so that the water reducing effect and the dispersing effect are enhanced; pollution and damage to the environment and the human body are prevented, meanwhile, direct cyclic utilization can be achieved, energy consumption is reduced, and secondary pollution and resource waste cannot be caused; the production cost of the water reducing agent or the dispersing agent is reduced.
本发明公开了一种1‑氨基蒽醌和DSD酸生产废水的资源化利用方法，所述方法包括如下步骤：步骤一，向反应釜中加入所述生产废水、磺化剂、苯酚、水、氢氧化钠，溶解搅拌混合均匀；步骤二，滴加丙酮，进行磺化反应，磺化反应结束后开始滴加甲醛溶液；步骤三，滴加完毕后进行保温；步骤四，保温结束即得混凝土减水剂或者水煤浆分散剂；所述步骤一中废水为1‑氨基蒽醌生产废水和DSD酸生产废水中的一种或者两种；对磺化丙酮甲醛缩合物或者氨基磺酸系甲醛缩合物进行接枝改性，增强了减水效果和分散效果；防止其对环境、对人体造成污染与损害，同时可直接循环利用，节省能耗，不会造成二次污染和资源的浪费；降低了减水剂或者分散剂的生产成本。
Resource utilization method of 1-aminoanthraquinone and DSD acid production wastewater
1-氨基蒽醌和DSD酸生产废水的资源化利用方法
DONG CUIPING (author) / MA LITAO (author) / YOU JIANJIAN (author) / YANG DAOSHUN (author) / LI MAN (author)
2020-10-27
Patent
Electronic Resource
Chinese
IPC:
C08G
MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
,
Makromolekulare Verbindungen, anders erhalten als durch Reaktionen, an denen nur ungesättigte Kohlenstoff-Kohlenstoff-Bindungen beteiligt sind
/
C04B
Kalk
,
LIME
/
C10L
FUELS NOT OTHERWISE PROVIDED FOR
,
Anderweitig nicht vorgesehene Brennstoffe
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