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Manufacturing method of transparent ceramic
The invention relates to a manufacturing method of bubble-defect-free transparent ceramic with high transmittance and uniform insertion loss in all in-plane areas. The method comprising the steps of: obtaining a candidate composition containing a binder, optionally a dispersant, and optionally a plasticizer; dissolving the candidate composition in a solvent, then reducing a contained solvent volume to 0.1% by mass or less, and measuring a glass transition temperature; selecting a candidate composition having a glass transition temperature of 25 C or more and 60 C or less as an organic additive composition; preparing the organic additive composition containing the binder, optionally the dispersant, and the plasticizer, and having the composition obtained in the selecting step; pulverizing a raw material for sintering formed from metal oxide powder and the organic additive composition to obtain a pulverized mixture; granulating the pulverized mixture; sintering the granulated mixture to obtain a sintered body; and pressurizing the sintered body.
一种具有高透射率且面内全部区域有均匀插入损失的无气泡缺陷的透明陶瓷的制造方法，包括如下工序：获得包含粘合剂并且任意选择地包含分散剂和/或增塑剂的候选组合物；将所述候选组合物溶解到溶剂中后使溶剂含量降低至0.1质量％以下并且测量玻璃化转变温度；将玻璃化转变温度为25℃以上且60℃以下的所述候选组合物选定为有机添加剂组合物；按所述选定的工序中得到的组成来制备包含所述粘合剂并且任意选择地包含分散剂和/或增塑剂的有机添加剂组合物；对由金属氧化物粉末形成的烧结用原料以及有机添加剂组合物进行粉碎获得粉碎混合物；对粉碎混合物进行颗粒化；对颗粒化后的混合物进行烧结得到烧结体；以及对烧结体进行加压。
Manufacturing method of transparent ceramic
The invention relates to a manufacturing method of bubble-defect-free transparent ceramic with high transmittance and uniform insertion loss in all in-plane areas. The method comprising the steps of: obtaining a candidate composition containing a binder, optionally a dispersant, and optionally a plasticizer; dissolving the candidate composition in a solvent, then reducing a contained solvent volume to 0.1% by mass or less, and measuring a glass transition temperature; selecting a candidate composition having a glass transition temperature of 25 C or more and 60 C or less as an organic additive composition; preparing the organic additive composition containing the binder, optionally the dispersant, and the plasticizer, and having the composition obtained in the selecting step; pulverizing a raw material for sintering formed from metal oxide powder and the organic additive composition to obtain a pulverized mixture; granulating the pulverized mixture; sintering the granulated mixture to obtain a sintered body; and pressurizing the sintered body.
一种具有高透射率且面内全部区域有均匀插入损失的无气泡缺陷的透明陶瓷的制造方法，包括如下工序：获得包含粘合剂并且任意选择地包含分散剂和/或增塑剂的候选组合物；将所述候选组合物溶解到溶剂中后使溶剂含量降低至0.1质量％以下并且测量玻璃化转变温度；将玻璃化转变温度为25℃以上且60℃以下的所述候选组合物选定为有机添加剂组合物；按所述选定的工序中得到的组成来制备包含所述粘合剂并且任意选择地包含分散剂和/或增塑剂的有机添加剂组合物；对由金属氧化物粉末形成的烧结用原料以及有机添加剂组合物进行粉碎获得粉碎混合物；对粉碎混合物进行颗粒化；对颗粒化后的混合物进行烧结得到烧结体；以及对烧结体进行加压。
Manufacturing method of transparent ceramic
透明陶瓷的制造方法
TANAKA KEITA (author)
2022-01-18
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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