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Preparation method of zirconium oxide wear-resistant particles
The invention discloses a preparation method of zirconium oxide wear-resistant particles, which comprises the following steps: putting zirconium oxide powder, deionized water, acrylamide, N, N-dimethyl bisacrylamide and ammonium polyacrylate into a ball milling tank, and carrying out ball milling to obtain low-viscosity slurry; preparing an ammonium persulfate aqueous solution, and uniformly mixing with silica gel; dropwise adding tetramethylethylenediamine into the slurry obtained by ball milling, and uniformly stirring; and sucking the slurry by using a 1ml dropper, dripping the slurry into silica gel, and forming to obtain the zirconium oxide wear-resistant particles. The particle size can be controlled according to the size of the dropper opening; in the preparation process, zirconia and alumina powder can be recovered and reused after loss, and the silica gel mold can be repeatedly used; the prepared zirconium oxide toughened aluminum oxide wear-resistant particles are better in wear-resistant effect and longer in service life.
本发明公开了一种氧化锆耐磨颗粒的制备方法,该方法包括以下步骤,将氧化锆粉末、去离子水、丙烯酰胺、N,N‑二甲基双丙烯酰胺、聚丙烯酸铵装入球磨罐中,经过球磨得到低黏度料浆;配制过硫酸铵水溶液与硅胶混合均;将四甲基乙二胺滴入球磨得到的料浆中,搅拌均匀;取1ml滴管吸入料浆,将料浆滴入硅胶中,成型得到氧化锆耐磨颗粒。本发明可以通过滴管口的大小来控制颗粒尺寸的大小;在制备过程中,出现的氧化锆、氧化铝粉末损失可以回收再次利用,硅胶模具可以重复使用;制备得到的氧化锆增韧氧化铝耐磨颗粒,耐磨效果更佳,使用寿命更长。
Preparation method of zirconium oxide wear-resistant particles
The invention discloses a preparation method of zirconium oxide wear-resistant particles, which comprises the following steps: putting zirconium oxide powder, deionized water, acrylamide, N, N-dimethyl bisacrylamide and ammonium polyacrylate into a ball milling tank, and carrying out ball milling to obtain low-viscosity slurry; preparing an ammonium persulfate aqueous solution, and uniformly mixing with silica gel; dropwise adding tetramethylethylenediamine into the slurry obtained by ball milling, and uniformly stirring; and sucking the slurry by using a 1ml dropper, dripping the slurry into silica gel, and forming to obtain the zirconium oxide wear-resistant particles. The particle size can be controlled according to the size of the dropper opening; in the preparation process, zirconia and alumina powder can be recovered and reused after loss, and the silica gel mold can be repeatedly used; the prepared zirconium oxide toughened aluminum oxide wear-resistant particles are better in wear-resistant effect and longer in service life.
本发明公开了一种氧化锆耐磨颗粒的制备方法,该方法包括以下步骤,将氧化锆粉末、去离子水、丙烯酰胺、N,N‑二甲基双丙烯酰胺、聚丙烯酸铵装入球磨罐中,经过球磨得到低黏度料浆;配制过硫酸铵水溶液与硅胶混合均;将四甲基乙二胺滴入球磨得到的料浆中,搅拌均匀;取1ml滴管吸入料浆,将料浆滴入硅胶中,成型得到氧化锆耐磨颗粒。本发明可以通过滴管口的大小来控制颗粒尺寸的大小;在制备过程中,出现的氧化锆、氧化铝粉末损失可以回收再次利用,硅胶模具可以重复使用;制备得到的氧化锆增韧氧化铝耐磨颗粒,耐磨效果更佳,使用寿命更长。
Preparation method of zirconium oxide wear-resistant particles
一种氧化锆耐磨颗粒的制备方法
XU KAI (Autor:in) / FENG ZHENGYANG (Autor:in) / JIANG YIXUAN (Autor:in) / CHEN JING (Autor:in) / YANG SUYAN (Autor:in) / TANG XIANYI (Autor:in)
27.10.2023
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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