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High-density high-purity carbon ceramic crucible and preparation method thereof
The invention discloses a high-density and high-purity carbon ceramic crucible and a preparation method thereof, and the method comprises the following steps: carrying out vapor deposition on a carbon fiber crucible preform to obtain a carbon-carbon composite crucible; the carbon-carbon composite crucible is sequentially subjected to carbon densification treatment, cracking after organic gel dipping, purification and impurity removal, silicon carbide layer coating treatment and ceramization treatment, and the carbon-carbon composite crucible is obtained. The method disclosed by the invention has the characteristic of simplicity and convenience in operation, and the production efficiency of the carbon-ceramic crucible is remarkably improved. The carbon-ceramic crucible prepared by the method is high in density, high in purity, excellent in mechanical property, high in corrosion resistance and long in service life.
本发明公开了一种高密高纯碳陶坩埚及其制备方法,该方法是将碳纤维坩埚预制体采用气相沉积碳,得到碳碳复合坩埚;再将碳碳复合坩埚依次进行增密碳处理、有机凝胶浸渍后裂解、纯化除杂、涂碳化硅层处理和陶瓷化处理,即得。本发明的方法具有操作简便的特点,显著提高了碳陶坩埚的生产效率。通过该方法制备的碳陶坩埚密度高、纯度高,机械性能优异,耐腐蚀性能强,使用寿命长。
High-density high-purity carbon ceramic crucible and preparation method thereof
The invention discloses a high-density and high-purity carbon ceramic crucible and a preparation method thereof, and the method comprises the following steps: carrying out vapor deposition on a carbon fiber crucible preform to obtain a carbon-carbon composite crucible; the carbon-carbon composite crucible is sequentially subjected to carbon densification treatment, cracking after organic gel dipping, purification and impurity removal, silicon carbide layer coating treatment and ceramization treatment, and the carbon-carbon composite crucible is obtained. The method disclosed by the invention has the characteristic of simplicity and convenience in operation, and the production efficiency of the carbon-ceramic crucible is remarkably improved. The carbon-ceramic crucible prepared by the method is high in density, high in purity, excellent in mechanical property, high in corrosion resistance and long in service life.
本发明公开了一种高密高纯碳陶坩埚及其制备方法,该方法是将碳纤维坩埚预制体采用气相沉积碳,得到碳碳复合坩埚;再将碳碳复合坩埚依次进行增密碳处理、有机凝胶浸渍后裂解、纯化除杂、涂碳化硅层处理和陶瓷化处理,即得。本发明的方法具有操作简便的特点,显著提高了碳陶坩埚的生产效率。通过该方法制备的碳陶坩埚密度高、纯度高,机械性能优异,耐腐蚀性能强,使用寿命长。
High-density high-purity carbon ceramic crucible and preparation method thereof
一种高密高纯碳陶坩埚及其制备方法
RONG GUANG (Autor:in) / LI JINWEI (Autor:in) / XIAO PENG (Autor:in)
13.02.2024
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
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