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Two-dimensional boron nitride full-ceramic fiber as well as preparation method and application thereof
The invention provides a two-dimensional boron nitride full-ceramic fiber and a preparation method and application thereof.The preparation method comprises the steps that a two-dimensional boron nitride dispersion liquid is provided and comprises two-dimensional boron nitride nanosheets and an organic solvent; adding an organic adhesive into the two-dimensional boron nitride dispersion liquid to obtain a mixed liquid; spinning the mixed solution by adopting wet spinning to obtain a gelatinous first fiber body; performing hot pressing on the first fiber body to obtain a second fiber body; pre-sintering the second fiber body in an oxygen-containing atmosphere to remove organic matters so as to obtain a precursor; in inert gas, Joule heat sintering is adopted for the precursor, and the two-dimensional boron nitride full-ceramic fiber is obtained.
本申请提供了一种二维氮化硼全陶瓷纤维、其制备方法及应用,所述制备方法包括:提供二维氮化硼分散液,所述二维氮化硼分散液包括二维氮化硼纳米片和有机溶剂;在所述二维氮化硼分散液中加入有机胶粘剂,得到混合液;采用湿法纺丝将所述混合液进行纺丝得到凝胶状的第一纤维体;对所述第一纤维体进行热压,得到第二纤维体;在含氧气氛中,对所述第二纤维体进行预烧结,以除去有机物,得到前驱体;在惰性气体中,采用焦耳热烧结所述前驱体,得到二维氮化硼全陶瓷纤维。
Two-dimensional boron nitride full-ceramic fiber as well as preparation method and application thereof
The invention provides a two-dimensional boron nitride full-ceramic fiber and a preparation method and application thereof.The preparation method comprises the steps that a two-dimensional boron nitride dispersion liquid is provided and comprises two-dimensional boron nitride nanosheets and an organic solvent; adding an organic adhesive into the two-dimensional boron nitride dispersion liquid to obtain a mixed liquid; spinning the mixed solution by adopting wet spinning to obtain a gelatinous first fiber body; performing hot pressing on the first fiber body to obtain a second fiber body; pre-sintering the second fiber body in an oxygen-containing atmosphere to remove organic matters so as to obtain a precursor; in inert gas, Joule heat sintering is adopted for the precursor, and the two-dimensional boron nitride full-ceramic fiber is obtained.
本申请提供了一种二维氮化硼全陶瓷纤维、其制备方法及应用,所述制备方法包括:提供二维氮化硼分散液,所述二维氮化硼分散液包括二维氮化硼纳米片和有机溶剂;在所述二维氮化硼分散液中加入有机胶粘剂,得到混合液;采用湿法纺丝将所述混合液进行纺丝得到凝胶状的第一纤维体;对所述第一纤维体进行热压,得到第二纤维体;在含氧气氛中,对所述第二纤维体进行预烧结,以除去有机物,得到前驱体;在惰性气体中,采用焦耳热烧结所述前驱体,得到二维氮化硼全陶瓷纤维。
Two-dimensional boron nitride full-ceramic fiber as well as preparation method and application thereof
二维氮化硼全陶瓷纤维、其制备方法及应用
QIU LING (Autor:in) / CHENG HUIMING (Autor:in) / DING SIYUAN (Autor:in) / LIU MINSU (Autor:in)
29.03.2024
Patent
Elektronische Ressource
Chinesisch
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