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C/C composite material anti-oxidation ablation coating prepared by utilizing polymer conversion ceramic as well as preparation method and application of C/C composite material anti-oxidation ablation coating
The invention discloses a C/C composite material anti-oxidation ablation coating prepared by utilizing polymer conversion ceramic as well as a preparation method and application of the C/C composite material anti-oxidation ablation coating, and relates to the technical field of surface coatings. The method comprises the following steps: preparing polymer converted ceramic powder; the preparation method comprises the following steps: uniformly mixing SiC powder in a phenolic resin ethanol solution to obtain slurry A; uniformly mixing SiC powder and polymer converted ceramic powder in a phenolic resin ethanol solution to obtain slurry B; sequentially coating the surface of the C/C composite material with the slurry A and the slurry B; and carrying out heat treatment on the C/C composite material with the pre-coating layer in an inert atmosphere to obtain the anti-oxidation ablation coating layer on the surface of the C/C composite material. The silicon-rich ceramic coating is prepared by introducing polymer converted superhigh-temperature ceramic into the surface of a C/C composite material by combining slurry coating with a high-temperature gas-phase siliconizing method. The preparation process is low in cost, simple, high in quality reliability and strong in designability.
本发明公开了一种利用聚合物转化陶瓷制备的C/C复合材料抗氧化烧蚀涂层及其制备方法和应用，涉及表面涂层技术领域。该方法包括制备聚合物转化陶瓷粉体；将SiC粉体均匀混合于酚醛树脂乙醇溶液中，获得浆料A；将SiC粉体以及聚合物转化陶瓷粉体均匀混合于酚醛树脂乙醇溶液中，获得浆料B；将浆料A、浆料B依次涂覆于C/C复合材料表面后；将带有预涂层的C/C复合材料，在惰性气氛中，进行热处理，即在C/C复合材料表面获得抗氧化烧蚀涂层。本发明通过料浆涂覆结合高温气相渗硅法将聚合物转化超高温陶瓷引入C/C复合材料表面制备得到富硅陶瓷涂层。其制备工艺成本低、工艺简单、质量可靠性高、可设计性强。
C/C composite material anti-oxidation ablation coating prepared by utilizing polymer conversion ceramic as well as preparation method and application of C/C composite material anti-oxidation ablation coating
The invention discloses a C/C composite material anti-oxidation ablation coating prepared by utilizing polymer conversion ceramic as well as a preparation method and application of the C/C composite material anti-oxidation ablation coating, and relates to the technical field of surface coatings. The method comprises the following steps: preparing polymer converted ceramic powder; the preparation method comprises the following steps: uniformly mixing SiC powder in a phenolic resin ethanol solution to obtain slurry A; uniformly mixing SiC powder and polymer converted ceramic powder in a phenolic resin ethanol solution to obtain slurry B; sequentially coating the surface of the C/C composite material with the slurry A and the slurry B; and carrying out heat treatment on the C/C composite material with the pre-coating layer in an inert atmosphere to obtain the anti-oxidation ablation coating layer on the surface of the C/C composite material. The silicon-rich ceramic coating is prepared by introducing polymer converted superhigh-temperature ceramic into the surface of a C/C composite material by combining slurry coating with a high-temperature gas-phase siliconizing method. The preparation process is low in cost, simple, high in quality reliability and strong in designability.
本发明公开了一种利用聚合物转化陶瓷制备的C/C复合材料抗氧化烧蚀涂层及其制备方法和应用，涉及表面涂层技术领域。该方法包括制备聚合物转化陶瓷粉体；将SiC粉体均匀混合于酚醛树脂乙醇溶液中，获得浆料A；将SiC粉体以及聚合物转化陶瓷粉体均匀混合于酚醛树脂乙醇溶液中，获得浆料B；将浆料A、浆料B依次涂覆于C/C复合材料表面后；将带有预涂层的C/C复合材料，在惰性气氛中，进行热处理，即在C/C复合材料表面获得抗氧化烧蚀涂层。本发明通过料浆涂覆结合高温气相渗硅法将聚合物转化超高温陶瓷引入C/C复合材料表面制备得到富硅陶瓷涂层。其制备工艺成本低、工艺简单、质量可靠性高、可设计性强。
C/C composite material anti-oxidation ablation coating prepared by utilizing polymer conversion ceramic as well as preparation method and application of C/C composite material anti-oxidation ablation coating
一种利用聚合物转化陶瓷制备的C/C复合材料抗氧化烧蚀涂层及其制备方法和应用
SUN JIA (author) / WANG YUQI (author) / HUANG SHIWEI (author) / ZHANG XUEMENG (author) / ZHANG YUYU (author) / GUO LINGXIANG (author) / FU QIANGANG (author)
2024-04-26
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
Preparation method of anti-oxidation ablation coating on surface of C/C composite material
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