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Preparation method of gallium and zirconium co-doped zinc oxide target material
The invention discloses a preparation method of a gallium and zirconium co-doped zinc oxide target material, and relates to the technical field of target materials, the preparation method comprises the following steps: S1, uniformly mixing zirconium oxide, gallium oxide, water and a dispersing agent, and grinding to obtain slurry I; s2, uniformly mixing zinc oxide, water and a dispersing agent, adding the slurry I, uniformly mixing, adding a binder and a plasticizer, uniformly mixing, and grinding to obtain slurry II; s3, performing spray drying and granulation on the slurry II, and sieving to obtain granular powder; s4, the granular powder is subjected to hydraulic pressure and cold isostatic pressing forming, and a plain blank is obtained; and S5, sintering the blank, and cooling to obtain the gallium-zirconium co-doped zinc oxide target material. The gallium and zirconium co-doped zinc oxide target material prepared by the preparation method disclosed by the invention has relatively high relative density and relatively low resistivity; after magnetron sputtering, the obtained film has good electrical properties.
本申请公开了一种镓和锆共掺杂氧化锌靶材的制备方法,涉及靶材技术领域,所述制备方法,包括如下步骤:S1:将氧化锆、氧化镓、水、分散剂混合均匀,研磨,得到浆料一;S2:将氧化锌、水、分散剂混合均匀后,加入浆料一,混合均匀,再加入粘结剂和增塑剂,混合均匀,研磨,得到浆料二;S3:对浆料二喷雾干燥造粒后,过筛,得到粒状粉料;S4:对粒状粉料液压、冷等静压成型,得到素胚;S5:对素胚进行烧结,冷却后,得到镓锆共掺杂氧化锌靶材。本申请制得的镓和锆共掺杂的氧化锌靶材具有较高的相对密度、较低的电阻率;磁控溅射后,获得的薄膜具有较好的电学性能。
Preparation method of gallium and zirconium co-doped zinc oxide target material
The invention discloses a preparation method of a gallium and zirconium co-doped zinc oxide target material, and relates to the technical field of target materials, the preparation method comprises the following steps: S1, uniformly mixing zirconium oxide, gallium oxide, water and a dispersing agent, and grinding to obtain slurry I; s2, uniformly mixing zinc oxide, water and a dispersing agent, adding the slurry I, uniformly mixing, adding a binder and a plasticizer, uniformly mixing, and grinding to obtain slurry II; s3, performing spray drying and granulation on the slurry II, and sieving to obtain granular powder; s4, the granular powder is subjected to hydraulic pressure and cold isostatic pressing forming, and a plain blank is obtained; and S5, sintering the blank, and cooling to obtain the gallium-zirconium co-doped zinc oxide target material. The gallium and zirconium co-doped zinc oxide target material prepared by the preparation method disclosed by the invention has relatively high relative density and relatively low resistivity; after magnetron sputtering, the obtained film has good electrical properties.
本申请公开了一种镓和锆共掺杂氧化锌靶材的制备方法,涉及靶材技术领域,所述制备方法,包括如下步骤:S1:将氧化锆、氧化镓、水、分散剂混合均匀,研磨,得到浆料一;S2:将氧化锌、水、分散剂混合均匀后,加入浆料一,混合均匀,再加入粘结剂和增塑剂,混合均匀,研磨,得到浆料二;S3:对浆料二喷雾干燥造粒后,过筛,得到粒状粉料;S4:对粒状粉料液压、冷等静压成型,得到素胚;S5:对素胚进行烧结,冷却后,得到镓锆共掺杂氧化锌靶材。本申请制得的镓和锆共掺杂的氧化锌靶材具有较高的相对密度、较低的电阻率;磁控溅射后,获得的薄膜具有较好的电学性能。
Preparation method of gallium and zirconium co-doped zinc oxide target material
一种镓和锆共掺杂氧化锌靶材的制备方法
YAO YUAN (author) / ZHANG LILAN (author) / ZHANG QIHUA (author) / HUANG SHICHENG (author) / LU YINGDONG (author) / ZHU YONGCHANG (author)
2025-01-03
Patent
Electronic Resource
Chinese
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