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Zinc oxide titanium yttrium powder, target material and preparation method of powder and target material
The invention belongs to the technical field of oxide target materials, and discloses zinc-titanium-yttrium oxide powder, a zinc-titanium-yttrium oxide target material and a preparation method of the zinc-titanium-yttrium oxide powder and the zinc-titanium-yttrium oxide target material, the preparation method comprises the following steps: step 1, mixing yttrium oxide powder, titanium oxide powder, pure water and a first dispersing agent, pre-dispersing, and performing wet grinding to obtain slurry I; 2, adding zinc oxide powder, pure water and a second dispersing agent into the slurry I, mixing, pre-dispersing, and performing wet grinding to obtain slurry II; 3, adding a binder into the slurry II, mixing, pre-dispersing, and performing wet grinding to obtain slurry III; 4, the third slurry is sequentially subjected to gas-water combined atomization granulation, mixing and screening, and zinc oxide titanium yttrium powder is obtained; wherein the gas atomization pressure of the gas-water combined atomization granulation in the step 4 is 0.6-0.8 MPa, and the included angle between the gas injection direction and the vertical downward direction is 30-50 degrees; the water pressure of water atomization is 50-150 MPa, and the included angle between the water spraying direction and the vertical downward direction is 30-50 degrees.
本发明属于氧化物靶材技术领域,公开了一种氧化锌钛钇粉体、靶材及粉体、靶材的制备方法,该制备方法包括如下步骤:步骤1:将氧化钇粉末、氧化钛粉末、纯水和第一分散剂经过混合、预分散后进行湿法研磨得到浆料一;步骤2:向浆料一中加入氧化锌粉末、纯水和第二分散剂经过混合、预分散后进行湿法研磨得到浆料二;步骤3:向浆料二中加入粘结剂经过混合、预分散后进行湿法研磨得到浆料三;步骤4:将浆料三依次进行气水联合雾化造粒、混料和筛分,得到氧化锌钛钇粉体;其中所述步骤4中气水联合雾化造粒的气雾化的气压为0.6‑0.8MPa,气体喷射方向与竖直向下方向的夹角为30‑50°;水雾化的水压为50‑150MPa,水的喷射方向与竖直向下方向的夹角为30‑50°。
Zinc oxide titanium yttrium powder, target material and preparation method of powder and target material
The invention belongs to the technical field of oxide target materials, and discloses zinc-titanium-yttrium oxide powder, a zinc-titanium-yttrium oxide target material and a preparation method of the zinc-titanium-yttrium oxide powder and the zinc-titanium-yttrium oxide target material, the preparation method comprises the following steps: step 1, mixing yttrium oxide powder, titanium oxide powder, pure water and a first dispersing agent, pre-dispersing, and performing wet grinding to obtain slurry I; 2, adding zinc oxide powder, pure water and a second dispersing agent into the slurry I, mixing, pre-dispersing, and performing wet grinding to obtain slurry II; 3, adding a binder into the slurry II, mixing, pre-dispersing, and performing wet grinding to obtain slurry III; 4, the third slurry is sequentially subjected to gas-water combined atomization granulation, mixing and screening, and zinc oxide titanium yttrium powder is obtained; wherein the gas atomization pressure of the gas-water combined atomization granulation in the step 4 is 0.6-0.8 MPa, and the included angle between the gas injection direction and the vertical downward direction is 30-50 degrees; the water pressure of water atomization is 50-150 MPa, and the included angle between the water spraying direction and the vertical downward direction is 30-50 degrees.
本发明属于氧化物靶材技术领域,公开了一种氧化锌钛钇粉体、靶材及粉体、靶材的制备方法,该制备方法包括如下步骤:步骤1:将氧化钇粉末、氧化钛粉末、纯水和第一分散剂经过混合、预分散后进行湿法研磨得到浆料一;步骤2:向浆料一中加入氧化锌粉末、纯水和第二分散剂经过混合、预分散后进行湿法研磨得到浆料二;步骤3:向浆料二中加入粘结剂经过混合、预分散后进行湿法研磨得到浆料三;步骤4:将浆料三依次进行气水联合雾化造粒、混料和筛分,得到氧化锌钛钇粉体;其中所述步骤4中气水联合雾化造粒的气雾化的气压为0.6‑0.8MPa,气体喷射方向与竖直向下方向的夹角为30‑50°;水雾化的水压为50‑150MPa,水的喷射方向与竖直向下方向的夹角为30‑50°。
Zinc oxide titanium yttrium powder, target material and preparation method of powder and target material
一种氧化锌钛钇粉体、靶材及粉体、靶材的制备方法
GU DESHENG (Autor:in) / SHAO XUELIANG (Autor:in) / LI KAIJIE (Autor:in) / ZHANG XINGYU (Autor:in) / LUO SISHI (Autor:in)
08.12.2023
Patent
Elektronische Ressource
Chinesisch
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