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Photo-curing 3D printing preparation method of black corundum-based TPMS heat absorption ceramic
The invention relates to the technical field of ceramic 3D printing, in particular to a black corundum-based TPMS heat absorption ceramic photocuring 3D printing preparation method which comprises the following steps: (1) dissolving black metal colorant ceramic powder and aluminum oxide ceramic powder in an aqueous solution containing fatty acid salt to obtain black metal ceramic powder coated with the aluminum oxide powder on the surface; (2) uniformly mixing the black metal ceramic powder coated with the aluminum oxide powder on the surface, aluminum oxide ceramic powder, light-cured resin, a dispersing agent and a photoinitiator to obtain composite ceramic slurry; and (3) designing a TPMS lattice structure from the composite ceramic slurry by utilizing 3D printing, and carrying out photocuring 3D printing, thermal degreasing and sintering to prepare the black corundum-based TPMS heat-absorbing ceramic. According to the scheme, the oxide-based heat-absorbing ceramic for solar thermal power generation is prepared by utilizing a photocuring 3D printing technology, and the technical problem that the oxide-based heat-absorbing ceramic for solar thermal power generation with complex shape and high absorptivity is difficult to prepare by a traditional forming method is solved.
本发明涉及陶瓷3D打印技术领域,具体涉及一种黑刚玉基TPMS吸热陶瓷的光固化3D打印制备方法,包括如下步骤:(1)将黑色金属着色剂陶瓷粉体和氧化铝陶瓷粉体溶于含有脂肪酸盐的水溶液中,获得表面包覆氧化铝粉体的黑色金属陶瓷粉体;(2)将表面包覆氧化铝粉体的黑色金属陶瓷粉体、氧化铝陶瓷粉体、光固化树脂、分散剂以及光引发剂混合均匀,获得复合陶瓷浆料;(3)将复合陶瓷浆料利用3D打印设计TPMS点阵结构,并通过光固化3D打印,经热脱脂和烧结后,制得黑刚玉基TPMS吸热陶瓷。上述方案利用光固化3D打印技术制备太阳能热发电用氧化物基吸热陶瓷,解决了传统成形方法难以制备复杂形状、高吸收率太阳能热发电用氧化物基吸热陶瓷的技术难题。
Photo-curing 3D printing preparation method of black corundum-based TPMS heat absorption ceramic
The invention relates to the technical field of ceramic 3D printing, in particular to a black corundum-based TPMS heat absorption ceramic photocuring 3D printing preparation method which comprises the following steps: (1) dissolving black metal colorant ceramic powder and aluminum oxide ceramic powder in an aqueous solution containing fatty acid salt to obtain black metal ceramic powder coated with the aluminum oxide powder on the surface; (2) uniformly mixing the black metal ceramic powder coated with the aluminum oxide powder on the surface, aluminum oxide ceramic powder, light-cured resin, a dispersing agent and a photoinitiator to obtain composite ceramic slurry; and (3) designing a TPMS lattice structure from the composite ceramic slurry by utilizing 3D printing, and carrying out photocuring 3D printing, thermal degreasing and sintering to prepare the black corundum-based TPMS heat-absorbing ceramic. According to the scheme, the oxide-based heat-absorbing ceramic for solar thermal power generation is prepared by utilizing a photocuring 3D printing technology, and the technical problem that the oxide-based heat-absorbing ceramic for solar thermal power generation with complex shape and high absorptivity is difficult to prepare by a traditional forming method is solved.
本发明涉及陶瓷3D打印技术领域,具体涉及一种黑刚玉基TPMS吸热陶瓷的光固化3D打印制备方法,包括如下步骤:(1)将黑色金属着色剂陶瓷粉体和氧化铝陶瓷粉体溶于含有脂肪酸盐的水溶液中,获得表面包覆氧化铝粉体的黑色金属陶瓷粉体;(2)将表面包覆氧化铝粉体的黑色金属陶瓷粉体、氧化铝陶瓷粉体、光固化树脂、分散剂以及光引发剂混合均匀,获得复合陶瓷浆料;(3)将复合陶瓷浆料利用3D打印设计TPMS点阵结构,并通过光固化3D打印,经热脱脂和烧结后,制得黑刚玉基TPMS吸热陶瓷。上述方案利用光固化3D打印技术制备太阳能热发电用氧化物基吸热陶瓷,解决了传统成形方法难以制备复杂形状、高吸收率太阳能热发电用氧化物基吸热陶瓷的技术难题。
Photo-curing 3D printing preparation method of black corundum-based TPMS heat absorption ceramic
一种黑刚玉基TPMS吸热陶瓷的光固化3D打印制备方法
YAN CHUNZE (Autor:in) / ZHOU SHIXIANG (Autor:in) / LIU GUIZHOU (Autor:in) / SHI YUSHENG (Autor:in)
15.03.2024
Patent
Elektronische Ressource
Chinesisch
IPC:
C04B
Kalk
,
LIME
/
B28B
Formgeben von Ton oder anderen keramischen Stoffzusammensetzungen, Schlacke oder von Mischungen, die zementartiges Material enthalten, z.B. Putzmörtel
,
SHAPING CLAY OR OTHER CERAMIC COMPOSITIONS, SLAG OR MIXTURES CONTAINING CEMENTITIOUS MATERIAL, e.g. PLASTER
/
B33Y
ADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
,
Additive (generative) Fertigung, d. h. die Herstellung von dreidimensionalen [3D] Bauteilen durch additive Abscheidung, additive Agglomeration oder additive Schichtung, z. B. durch 3D- Drucken, Stereolithografie oder selektives Lasersintern
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