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Silicon nitride nanowire/calcium phosphate ceramic non-combustible paper and preparation method thereof
The invention discloses silicon nitride nanowire/calcium phosphate ceramic non-combustible paper and a preparation method thereof. The preparation method comprises the following steps: 1) obtaining a solution A; 2) standing and curing the solution A, and then grinding into powder B; (3) the powder B obtained in the step (2) is evenly laid in a substrate, then the substrate is placed in a heating furnace to be subjected to heat treatment, after furnace cooling is conducted, an obtained product is stripped from the surface of the substrate, and a sample C is obtained; 4) putting the sample C into a chemical vapor deposition furnace, heating, introducing natural gas and argon, and preserving heat to obtain a sample D; 5) obtaining a solution E; 6) carrying out electrolytic deposition by using a graphite plate as an anode, the sample D as a cathode and the solution E as an electrolyte to obtain a sample F; and 7) placing the sample F in an oxidation furnace, carrying out oxidation treatment in an air atmosphere, and cooling to obtain the silicon nitride nanowire/calcium phosphate ceramic non-combustible paper, the non-combustible paper prepared by the method has excellent acid and alkali corrosion resistance and fire resistance, and has a heat insulation effect.
本发明公开了一种氮化硅纳米线/钙磷陶瓷不燃纸及其制备方法，包括以下步骤：1)得溶液A；2)将溶液A静置固化，然后研磨成粉末B；3)将步骤2)得到的粉末B均匀平铺在基板中，再置于加热炉中进行热处理，再随炉冷却后，将所得产物从基板表面剥离，得样品C；4)将样品C放入化学气相沉积炉中，再升温，然后通入天然气及氩气，并保温，得样品D；5)得到溶液E；6)采用石墨板作为阳极，样品D作为阴极，溶液E为电解液，进行电解沉积，得到样品F；7)将样品F置于氧化炉中，在空气氛围中氧化处理，冷却后，得氮化硅纳米线/钙磷陶瓷不燃纸，该方法制备得到的不燃纸的耐酸碱腐蚀性能及耐火性能优异，且具有隔热效果。
Silicon nitride nanowire/calcium phosphate ceramic non-combustible paper and preparation method thereof
The invention discloses silicon nitride nanowire/calcium phosphate ceramic non-combustible paper and a preparation method thereof. The preparation method comprises the following steps: 1) obtaining a solution A; 2) standing and curing the solution A, and then grinding into powder B; (3) the powder B obtained in the step (2) is evenly laid in a substrate, then the substrate is placed in a heating furnace to be subjected to heat treatment, after furnace cooling is conducted, an obtained product is stripped from the surface of the substrate, and a sample C is obtained; 4) putting the sample C into a chemical vapor deposition furnace, heating, introducing natural gas and argon, and preserving heat to obtain a sample D; 5) obtaining a solution E; 6) carrying out electrolytic deposition by using a graphite plate as an anode, the sample D as a cathode and the solution E as an electrolyte to obtain a sample F; and 7) placing the sample F in an oxidation furnace, carrying out oxidation treatment in an air atmosphere, and cooling to obtain the silicon nitride nanowire/calcium phosphate ceramic non-combustible paper, the non-combustible paper prepared by the method has excellent acid and alkali corrosion resistance and fire resistance, and has a heat insulation effect.
本发明公开了一种氮化硅纳米线/钙磷陶瓷不燃纸及其制备方法，包括以下步骤：1)得溶液A；2)将溶液A静置固化，然后研磨成粉末B；3)将步骤2)得到的粉末B均匀平铺在基板中，再置于加热炉中进行热处理，再随炉冷却后，将所得产物从基板表面剥离，得样品C；4)将样品C放入化学气相沉积炉中，再升温，然后通入天然气及氩气，并保温，得样品D；5)得到溶液E；6)采用石墨板作为阳极，样品D作为阴极，溶液E为电解液，进行电解沉积，得到样品F；7)将样品F置于氧化炉中，在空气氛围中氧化处理，冷却后，得氮化硅纳米线/钙磷陶瓷不燃纸，该方法制备得到的不燃纸的耐酸碱腐蚀性能及耐火性能优异，且具有隔热效果。
Silicon nitride nanowire/calcium phosphate ceramic non-combustible paper and preparation method thereof
一种氮化硅纳米线/钙磷陶瓷不燃纸及其制备方法
ZHANG LEILEI (author) / LI HAIYANG (author) / SONG QIANG (author) / LI HEJUN (author)
2024-04-09
Patent
Electronic Resource
Chinese
IPC:
C04B
Kalk
,
LIME
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