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METHOD FOR MANUFACTURING SILICON NITRIDE SINTERED COMPACT
The present invention is directed to a method for producing a silicon nitride sintered material, the method including heating a molded article, which contains a silicon nitride powder having a β phase ratio of 80% or more, a dissolved oxygen content of 0.2% by mass or less, and a specific surface area of 5 to 20 m2/g, and a sintering auxiliary containing a compound having no oxygen bond, and which has an overall oxygen content controlled to be 1 to 15% by mass and an aluminum element overall content controlled to be 800 ppm or less, to a temperature of 1,200 to 1,800° C. in an inert gas atmosphere under a pressure of 0 MPa·G or more and less than 0.1 MPa·G to sinter the silicon nitride.In the present invention, there can be provided a method for producing a silicon nitride sintered material, which method is advantageous in that a silicon nitride sintered material having high thermal conductivity can be obtained even when using a silicon nitride powder having a high β phase ratio and conducting calcination under normal pressure or substantially normal pressure.
METHOD FOR MANUFACTURING SILICON NITRIDE SINTERED COMPACT
The present invention is directed to a method for producing a silicon nitride sintered material, the method including heating a molded article, which contains a silicon nitride powder having a β phase ratio of 80% or more, a dissolved oxygen content of 0.2% by mass or less, and a specific surface area of 5 to 20 m2/g, and a sintering auxiliary containing a compound having no oxygen bond, and which has an overall oxygen content controlled to be 1 to 15% by mass and an aluminum element overall content controlled to be 800 ppm or less, to a temperature of 1,200 to 1,800° C. in an inert gas atmosphere under a pressure of 0 MPa·G or more and less than 0.1 MPa·G to sinter the silicon nitride.In the present invention, there can be provided a method for producing a silicon nitride sintered material, which method is advantageous in that a silicon nitride sintered material having high thermal conductivity can be obtained even when using a silicon nitride powder having a high β phase ratio and conducting calcination under normal pressure or substantially normal pressure.
METHOD FOR MANUFACTURING SILICON NITRIDE SINTERED COMPACT
MABUCHI TOSHIROU (author) / WAKAMATSU SATORU (author)
2022-12-22
Patent
Electronic Resource
English
IPC:
C04B
Kalk
,
LIME
METHOD FOR MANUFACTURING SILICON NITRIDE SINTERED COMPACT
| European Patent Office | 2021
METHOD FOR MANUFACTURING SILICON NITRIDE SINTERED COMPACT
| European Patent Office | 2024